ethyl α-<(triphenylphosphoranylidene)amino>-2-(allyloxy)-3-methoxycinnamate

Base Information

Chemical Name:ethyl α-<(triphenylphosphoranylidene)amino>-2-(allyloxy)-3-methoxycinnamate
CAS No.:133495-73-5
Molecular Formula:C₃₃H₃₂NO₄P
Molecular Weight:537.595
Hs Code.:

Synonyms:ethyl α-<(triphenylphosphoranylidene)amino>-2-(allyloxy)-3-methoxycinnamate

Suppliers and Price of ethyl α-<(triphenylphosphoranylidene)amino>-2-(allyloxy)-3-methoxycinnamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of ethyl α-<(triphenylphosphoranylidene)amino>-2-(allyloxy)-3-methoxycinnamate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of ethyl α-<(triphenylphosphoranylidene)amino>-2-(allyloxy)-3-methoxycinnamate

There total 3 articles about ethyl α-<(triphenylphosphoranylidene)amino>-2-(allyloxy)-3-methoxycinnamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 127983-47-5
ethyl α-azido-2-(allyloxy)-3-methoxy-cinnamate

: 603-35-0
triphenylphosphine

: 133495-73-5
ethyl α-<(triphenylphosphoranylidene)amino>-2-(allyloxy)-3-methoxycinnamate

Guidance literature:: In diethyl ether; Ambient temperature;
DOI:10.1039/c39900000007

Reference yield:

: 23343-06-8
2-allyloxy-3-methoxy-benzaldehyde

: 133495-73-5
ethyl α-<(triphenylphosphoranylidene)amino>-2-(allyloxy)-3-methoxycinnamate

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / NaOEt / ethanol / 3 h / -20 °C

2: 90 percent / diethyl ether / 12 h / Ambient temperature

With sodium ethanolate; In diethyl ether; ethanol;
DOI:10.1021/jo00312a020

Reference yield:

: 148-53-8
3-methoxy-2-hydroxybenzaldehyde

: 133495-73-5
ethyl α-<(triphenylphosphoranylidene)amino>-2-(allyloxy)-3-methoxycinnamate

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / K₂CO₃ / acetone / Heating

2: 60 percent / NaOEt / ethanol / -15 °C

3: 90 percent / diethyl ether / Ambient temperature

With sodium ethanolate; potassium carbonate; In diethyl ether; ethanol; acetone;
DOI:10.1039/c39900000007