phosphoric acid dibenzyl ester 2,3-bis-benzyloxy-4-(tert-butyl-dimethyl-silanyloxy)-butyl ester

Base Information

Chemical Name:phosphoric acid dibenzyl ester 2,3-bis-benzyloxy-4-(tert-butyl-dimethyl-silanyloxy)-butyl ester
CAS No.:926919-29-1
Molecular Formula:C₃₈H₄₉O₇PSi
Molecular Weight:676.862
Hs Code.:

phosphoric acid dibenzyl ester 2,3-bis-benzyloxy-4-(<i>tert</i>-butyl-dimethyl-silanyloxy)-butyl ester

Synonyms:phosphoric acid dibenzyl ester 2,3-bis-benzyloxy-4-(tert-butyl-dimethyl-silanyloxy)-butyl ester

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Chemical Property of phosphoric acid dibenzyl ester 2,3-bis-benzyloxy-4-(tert-butyl-dimethyl-silanyloxy)-butyl ester

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Technology Process of phosphoric acid dibenzyl ester 2,3-bis-benzyloxy-4-(tert-butyl-dimethyl-silanyloxy)-butyl ester

There total 3 articles about phosphoric acid dibenzyl ester 2,3-bis-benzyloxy-4-(tert-butyl-dimethyl-silanyloxy)-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 67746-43-4
dibenzyl N,N-diethylphosphoramidite

: 171622-74-5
(2R,3R)-2,3-bis(benzyloxy)-4-((tert-butyldimethylsilyl)oxy)butan-1-ol

: 926919-29-1
phosphoric acid dibenzyl ester 2,3-bis-benzyloxy-4-(tert-butyl-dimethyl-silanyloxy)-butyl ester

Guidance literature:: With 1H-tetrazole; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1016/j.tetlet.2006.11.091

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 926919-29-1
phosphoric acid dibenzyl ester 2,3-bis-benzyloxy-4-(tert-butyl-dimethyl-silanyloxy)-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / NaH / tetrahydrofuran

2: 81 percent / tetrazole; mCPBA / CH₂Cl₂

With 1H-tetrazole; sodium hydride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tetlet.2006.11.091

Reference yield:

: 113350-84-8
(2R,3R)-(-)-2,3-bis(phenylmethoxy)-1,4-butanediol

: 926919-29-1
phosphoric acid dibenzyl ester 2,3-bis-benzyloxy-4-(tert-butyl-dimethyl-silanyloxy)-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / NaH / tetrahydrofuran

2: 81 percent / tetrazole; mCPBA / CH₂Cl₂

With 1H-tetrazole; sodium hydride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tetlet.2006.11.091