2-[2-(2-Undec-10-enoxyethoxy)ethoxy]ethanol

Base Information

• Chemical Name: 2-[2-(2-Undec-10-enoxyethoxy)ethoxy]ethanol
• CAS No.: 130727-45-6
• Molecular Formula: C17H34 O4
• Molecular Weight: 302.455
• European Community (EC) Number: 631-333-5
• DSSTox Substance ID: DTXSID00394375
• Wikidata: Q82193715
• Mol file: 130727-45-6.mol

Synonyms:130727-45-6;3,6,9-TRIOXAEICOS-19-EN-1-OL;2-[2-(2-undec-10-enoxyethoxy)ethoxy]ethanol;Ethanol, 2-[2-[2-(10-undecen-1-yloxy)ethoxy]ethoxy]-;SCHEMBL826393;DTXSID00394375;SNQQBXFXPDCEIT-UHFFFAOYSA-N;MFCD03425658;AKOS030240287;FT-0675653;2-[2-(2-Undec-10-enyloxyethoxy)ethoxy]ethanol;J-005863;2-(2-{2-[(Undec-10-en-1-yl)oxy]ethoxy}ethoxy)ethan-1-ol

Chemical Property of 2-[2-(2-Undec-10-enoxyethoxy)ethoxy]ethanol

Chemical Property:

• Vapor Pressure: 7.32E-08mmHg at 25°C
• Refractive Index: 1.456
• Boiling Point: 394.6°C at 760 mmHg
• Flash Point: 192.4°C
• PSA: 47.92000
• Density: 0.942g/cm³
• LogP: 3.33530
• Solubility.: Chloroform, Dichloromethane, Ethyl Acetate, Methanol
• XLogP3: 3.7
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 18
• Exact Mass: 302.24570956
• Heavy Atom Count: 21
• Complexity: 197

Purity/Quality:

98%Min ^*data from raw suppliers

3,6,9-Trioxaeicos-19-en-1-ol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C=CCCCCCCCCCOCCOCCOCCO
• Uses: 3,6,9-Trioxaeicos-19-en-1-ol (cas# 130727-45-6) is a compound useful in organic synthesis.

Technology Process of 2-[2-(2-Undec-10-enoxyethoxy)ethoxy]ethanol

There total 2 articles about 2-[2-(2-Undec-10-enoxyethoxy)ethoxy]ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

1-undecen-11-ylbromide (7766-50-9) + 2,2'-[1,2-ethanediylbis(oxy)]bisethanol (112-27-6) → 2-(2-(2-(undec-10-enyloxy)ethoxy)ethoxy)ethanol (130727-45-6)

Guidance literature:

2,2'-[1,2-ethanediylbis(oxy)]bisethanol; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;

1-undecen-11-ylbromide; In N,N-dimethyl-formamide; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1002/chem.200902693

Reference yield: 74.0%

1-undecen-11-ylbromide (7766-50-9) + 2,2'-[1,2-ethanediylbis(oxy)]bisethanol (112-27-6) → C28H54O4 (700847-04-7) + 2-(2-(2-(undec-10-enyloxy)ethoxy)ethoxy)ethanol (130727-45-6)

Guidance literature:

2,2'-[1,2-ethanediylbis(oxy)]bisethanol; With sodium hydroxide; In water; at 100 ℃; for 0.5h; Inert atmosphere;

1-undecen-11-ylbromide; at 100 ℃; for 24h; Inert atmosphere;

DOI:10.1039/b919347b

Reference yield: 100.0%

2-(2-(2-(undec-10-enyloxy)ethoxy)ethoxy)ethanol (130727-45-6) + tiolacetic acid (507-09-5) → <1-<(methylcarbonyl)thio>undec-11-yl>tri(ethylene glycol) (130727-50-3)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); In tetrahydrofuran; at 20 ℃; for 3h; Inert atmosphere; UV-irradiation;

DOI:10.1002/chem.200902693

upstream raw materials:

1-undecen-11-ylbromide

2,2'-[1,2-ethanediylbis(oxy)]bisethanol

Downstream raw materials:

<1-<(methylcarbonyl)thio>undec-11-yl>tri(ethylene glycol)

(1-mercaptoundec-11-yl)tri(ethylene glycol)