(SP)-(-)-N-METHYL-N-[(1R,2S)-(2-HYDROXY-1-METHYL-2-PHENYL)ETHYL]AMINO-O-ANIYSYLPHENYLPHOSPHINE

Base Information

Chemical Name:(SP)-(-)-N-METHYL-N-[(1R,2S)-(2-HYDROXY-1-METHYL-2-PHENYL)ETHYL]AMINO-O-ANIYSYLPHENYLPHOSPHINE
CAS No.:131766-47-7
Molecular Formula:C₂₃H₂₉BNO₂P
Molecular Weight:393.274
Hs Code.:
Mol file:131766-47-7.mol

Synonyms:(SP)-(-)-N-METHYL-N-[(1R,2S)-(2-HYDROXY-1-METHYL-2-PHENYL)ETHYL]AMINO-O-ANIYSYLPHENYLPHOSPHINE;(RP)-(-)-N-METHYL-N-[(1R,2S)-(2-HYDROXY-1-METHYL-2-PHENYL)ETHYL]AMINO-O-ANIYSYLPHENYLPHOSPHINE

Suppliers and Price of (SP)-(-)-N-METHYL-N-[(1R,2S)-(2-HYDROXY-1-METHYL-2-PHENYL)ETHYL]AMINO-O-ANIYSYLPHENYLPHOSPHINE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
(SP)-(-)-N-METHYL-N-[(1R,2S)-(2-HYDROXY-1-METHYL-2-PHENYL)ETHYL]AMINO-ORTHO-ANIYSYLPHENYLPHOSPHINE 95.00%
5MG
$ 503.03

Total 3 raw suppliers

Chemical Property of (SP)-(-)-N-METHYL-N-[(1R,2S)-(2-HYDROXY-1-METHYL-2-PHENYL)ETHYL]AMINO-O-ANIYSYLPHENYLPHOSPHINE

Chemical Property:

PSA：46.29000
LogP:4.09680

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

(SP)-(-)-N-METHYL-N-[(1R,2S)-(2-HYDROXY-1-METHYL-2-PHENYL)ETHYL]AMINO-ORTHO-ANIYSYLPHENYLPHOSPHINE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (SP)-(-)-N-METHYL-N-[(1R,2S)-(2-HYDROXY-1-METHYL-2-PHENYL)ETHYL]AMINO-O-ANIYSYLPHENYLPHOSPHINE

There total 1 articles about (SP)-(-)-N-METHYL-N-[(1R,2S)-(2-HYDROXY-1-METHYL-2-PHENYL)ETHYL]AMINO-O-ANIYSYLPHENYLPHOSPHINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: (2S,4S,5R)-(+)-3,4-dimethyl-2,5-diphenyl-1,3,2-oxaazaphospholidine-2-borane

: 7732-18-5
water

: 31600-86-9
2-methoxyphenyllithium

: 131766-47-7,264871-34-3,1071028-70-0,227314-62-7
HOCH(C₆H₅)CH(CH₃)N(CH₃)P(BH₃)(C₆H₅)C₆H₄OCH₃

Guidance literature:: In tetrahydrofuran; N2-atmosphere; stirring (-40°C, 1 h), H2O addn. (0°C); evapn., CH2Cl2 addn., chromy. (SiO2, Et2O), evapn. (vac.);
DOI:10.1021/om960982+

Reference yield: 80.0%

: 67-56-1
methanol

: 131766-47-7,264871-34-3,1071028-70-0,227314-62-7
HOCH(C₆H₅)CH(CH₃)N(CH₃)P(BH₃)(C₆H₅)C₆H₄OCH₃

: methyl (S)-(-)-(2-methoxyphenyl)phenylphosphinite borane complex

Guidance literature:: With H₂SO₄; In methanol; N2-atmosphere; stirring (overnight); filtering, evapn. (vac.), extg. (CH2Cl2), chromy., evapn. (vac.); elem. anal.;
DOI:10.1021/om960982+