BIPHENYLDIISOPROPYLSILYL CHLORIDE

Base Information

Chemical Name:BIPHENYLDIISOPROPYLSILYL CHLORIDE
CAS No.:136449-55-3
Molecular Formula:C18H23ClSi
Molecular Weight:302.91
Hs Code.:2931900090
Mol file:136449-55-3.mol

Synonyms:CHLOROBIPHENYLBIS(1-METHYLETHYL)SILANE;BIPHENYLDIISOPROPYLSILYL CHLORIDE;P-BIPHENYL-DIISOPROPYLSILYL CHLORIDE

Suppliers and Price of BIPHENYLDIISOPROPYLSILYL CHLORIDE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
BIPHENYLDIISOPROPYLSILYL CHLORIDE 95.00%
1G
$ 1067.22

Total 3 raw suppliers

Chemical Property of BIPHENYLDIISOPROPYLSILYL CHLORIDE

Chemical Property:

PSA：0.00000
LogP:5.56490
Storage Temp.:0-6°C

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

BIPHENYLDIISOPROPYLSILYL CHLORIDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:C
Statements: 34-29
Safety Statements: 45-36/37/39-26

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of BIPHENYLDIISOPROPYLSILYL CHLORIDE

There total 5 articles about BIPHENYLDIISOPROPYLSILYL CHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 136449-69-9
[1,1′-biphenyl]-4-yldiisopropylsilane

: 136449-55-3
biphenyldiisopropylsilyl chloride

Guidance literature:: With copper dichloride; In acetonitrile; for 18h; Heating;
DOI:10.1016/S0040-4039(00)79376-2

Reference yield:

: 7751-38-4
Diisopropylsilyl dichloride

: 92-66-0
4-bromo-1,1'-biphenyl

: 136449-55-3
biphenyldiisopropylsilyl chloride

Guidance literature:: 4-bromo-1,1'-biphenyl; With n-butyllithium; In diethyl ether; hexane; at 0 ℃; for 1h; Inert atmosphere;

Diisopropylsilyl dichloride; In diethyl ether; hexane; at -73 - 20 ℃; for 8h; Inert atmosphere;
DOI:10.1039/c6ob00674d

Reference yield:

: 1201-71-4
4-biphenyllithium

: 136449-55-3
biphenyldiisopropylsilyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 1) Cl₃SiH / 1) Et₂O, 20 deg C, 16 h, 2a) Et₂O, hexane, 2b) 16 h

2: 91 percent / CuCl₂ / acetonitrile / 18 h / Heating

With trichlorosilane; copper dichloride; In acetonitrile;
DOI:10.1016/S0040-4039(00)79376-2