alpha-D-erythro-Pentofuranosiduronicacid,methyl2,3-dideoxy-3-nitro-,methylester(9CI)

Base Information

• Chemical Name: alpha-D-erythro-Pentofuranosiduronicacid,methyl2,3-dideoxy-3-nitro-,methylester(9CI)
• CAS No.: 136572-24-2
• Molecular Formula: C7H11NO6
• Molecular Weight: 205.17
• Mol file: 136572-24-2.mol

Synonyms:alpha-D-erythro-Pentofuranosiduronicacid,methyl2,3-dideoxy-3-nitro-,methylester(9CI)

Chemical Property of alpha-D-erythro-Pentofuranosiduronicacid,methyl2,3-dideoxy-3-nitro-,methylester(9CI)

Chemical Property:

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Technology Process of alpha-D-erythro-Pentofuranosiduronicacid,methyl2,3-dideoxy-3-nitro-,methylester(9CI)

There total 9 articles about alpha-D-erythro-Pentofuranosiduronicacid,methyl2,3-dideoxy-3-nitro-,methylester(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

methanol (67-56-1) + 2-hydroxy-3-nitro-5-oxopentanoic acid ethylene acetal (93715-55-0,93715-56-1) → methyl (methyl 2,3-dideoxy-3-nitro-α-DL-ribofuranosid)uronate (93715-68-5,136572-24-2) + methyl (methyl 2,3-dideoxy-3-nitro-β-DL-ribofuranosid)uronate (93715-67-4,136572-24-2) + methyl (methyl 2,3-dideoxy-3-nitro-α-DL-xylofuranosid)uronate (93715-69-6,136572-24-2)

Guidance literature:

With hydrogenchloride; for 24h; Ambient temperature;

DOI:10.1021/jo00201a018

Reference yield: 22.0%

methanol (67-56-1) + 2-hydroxy-3-nitro-5-oxopentanoic acid ethylene acetal (93715-55-0,93715-56-1) → methyl (methyl 2,3-dideoxy-3-nitro-α-DL-ribofuranosid)uronate (93715-68-5,136572-24-2) + methyl (methyl 2,3-dideoxy-3-nitro-β-DL-ribofuranosid)uronate (93715-67-4,136572-24-2) + methyl (methyl 2,3-dideoxy-3-nitro-α-DL-xylofuranosid)uronate (93715-69-6,136572-24-2)

Guidance literature:

With hydrogenchloride; for 24h; Ambient temperature;

DOI:10.1021/jo00201a018

Reference yield: 22.0%

methanol (67-56-1) + 2-hydroxy-3-nitro-5-oxopentanoic acid ethylene acetal (93715-55-0,93715-56-1) → methyl (methyl 2,3-dideoxy-3-nitro-α-DL-ribofuranosid)uronate (93715-68-5,136572-24-2) + methyl (methyl 2,3-dideoxy-3-nitro-β-DL-ribofuranosid)uronate (93715-67-4,136572-24-2) + methyl (methyl 2,3-dideoxy-3-nitro-α-DL-xylofuranosid)uronate (93715-69-6,136572-24-2)

Guidance literature:

With hydrogenchloride; for 24h; Ambient temperature;

DOI:10.1021/jo00201a018

upstream raw materials:

(2S,5R)-5-Methoxy-3-nitro-2,5-dihydro-furan-2-carboxylic acid methyl ester

3-deoxy-1,2:5,6-di-O-isopropylidene-3-nitro-α-D-allofuranose

(E/Z)-3-Deoxy-3-hydroxyimino-1,2:5,6-di-O-isopropylidene-α-D-ribohexofuranose

3-deoxy-1,2-O-isopropylidene-3-nitro-α-D-ribofuranosuronic acid

Downstream raw materials:

methyl 2,3-dideoxy-3-nitro-β-D-erythro-pentofuranosiduronic acid

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