1,3-Dioxolane-4,5-dicarboxaldehyde, 2,2-dimethyl-, cis- (9CI)

Base Information

Chemical Name:1,3-Dioxolane-4,5-dicarboxaldehyde, 2,2-dimethyl-, cis- (9CI)
CAS No.:146566-82-7
Molecular Formula:C7H10 O4
Molecular Weight:158.154
Hs Code.:
Mol file:146566-82-7.mol

Synonyms:1,3-Dioxolane-4,5-dicarboxaldehyde, 2,2-dimethyl-, cis- (9CI)

Suppliers and Price of 1,3-Dioxolane-4,5-dicarboxaldehyde, 2,2-dimethyl-, cis- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 1,3-Dioxolane-4,5-dicarboxaldehyde, 2,2-dimethyl-, cis- (9CI)

Chemical Property:

PSA：52.60000
LogP:-0.09570

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1,3-Dioxolane-4,5-dicarboxaldehyde, 2,2-dimethyl-, cis- (9CI)

There total 17 articles about 1,3-Dioxolane-4,5-dicarboxaldehyde, 2,2-dimethyl-, cis- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 3969-84-4,33493-69-5,94925-98-1
3,4-O-isopropylidene-D-mannitol

: 5754-27-8,85362-89-6,122137-20-6,146566-82-7
(4S,5S)-2,2-dimethyl-[1,3]dioxolane-4,5-dicarbaldehyde

Guidance literature:: With sodium periodate; In methanol; at 0 - 20 ℃; for 1h; phosphate buffer (pH 7.13);
DOI:10.1016/S0040-4020(01)80130-7

Reference yield:

: 50-70-4
D-sorbitol

: 67-64-1
acetone

: 97718-39-3
2,3-O-isopropylidene-L-threose

: 146566-82-7
(4R,5S)-2,2-dimethyl-1,3-dioxolane-4,5-dicarbaldehyde

: 15186-48-8
2,3-isopropylidene-glyceraldehyde

Guidance literature:: With sodium periodate; Dowex 50W(H⁽¹⁺⁾) resin; sodium hydrogencarbonate; Multistep reaction. Title compound not separated from byproducts; 1.) DMF, RT, 24 h; 2.) H₂O, RT, 1 h;
DOI:10.1016/0008-6215(85)85116-8

Reference yield:

: 50-70-4
D-sorbitol

: 77-76-9
2,2-dimethoxy-propane

: 97718-39-3
2,3-O-isopropylidene-L-threose

: 146566-82-7
(4R,5S)-2,2-dimethyl-1,3-dioxolane-4,5-dicarbaldehyde

: 97672-51-0,255840-20-1
2,4-O-isopropylidene-D-threose

: 15186-48-8
2,3-isopropylidene-glyceraldehyde

Guidance literature:: With sodium periodate; sodium hydrogencarbonate; toluene-4-sulfonic acid; Multistep reaction. Further byproducts given. Title compound not separated from byproducts; 1.) DMF, RT, 1 h; 2.) H₂O, RT, 1 h;
DOI:10.1016/0008-6215(85)85116-8