1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluoro-8,8-dimethoxyoctane

Base Information

• Chemical Name: 1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluoro-8,8-dimethoxyoctane
• CAS No.: 142502-76-9
• Molecular Formula: C₁₀H₉F₁₃O₂
• Molecular Weight: 408.159
• Hs Code.: 2912120000
• DSSTox Substance ID: DTXSID30379852
• Wikidata: Q82169867
• Mol file: 142502-76-9.mol

Synonyms:142502-76-9;1,1,1,2,2,3,3,4,4,5,5,6,6-tridecafluoro-8,8-dimethoxyoctane;2-(Perfluorohexyl)acetaldehyde dimethyl acetal;2-(Perfluoro-n-hexyl)acetaldehyde dimethyl acetal;SCHEMBL5704634;DTXSID30379852;AKOS015851428;FT-0608899;A807920;1,1,1,2,2,3,3,4,4,5,5,6,6-tridecakis(fluoranyl)-8,8-dimethoxy-octane

Chemical Property of 1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluoro-8,8-dimethoxyoctane

Chemical Property:

• Vapor Pressure: 1.94mmHg at 25°C
• Refractive Index: 1.311
• Boiling Point: 170.5°Cat760mmHg
• Flash Point: 63.1°C
• PSA: 18.46000
• Density: 1.469g/cm³
• LogP: 4.73420
• Storage Temp.: 2-8°C
• XLogP3: 4.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 15
• Rotatable Bond Count: 8
• Exact Mass: 408.0394956
• Heavy Atom Count: 25
• Complexity: 452

Purity/Quality:

97% ^*data from raw suppliers

2-(Perfluorohexyl)acetaldehyde dimethyl acetal 97% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36

MSDS Files:

Useful:

• Canonical SMILES: COC(CC(C(C(C(C(C(F)(F)F)(F)F)(F)F)(F)F)(F)F)(F)F)OC

Technology Process of 1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluoro-8,8-dimethoxyoctane

There total 4 articles about 1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluoro-8,8-dimethoxyoctane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

(Z)-2-tridecafluorohexyl-1-methoxyethylene + methanol (67-56-1) → 2-tridecafluorohexyl-1,1-dimethoxyethane (142502-76-9)

Guidance literature:

With toluene-4-sulfonic acid; In dichloromethane; at 40 ℃; for 24h;

DOI:10.1016/j.jfluchem.2004.07.001

Reference yield:

n-perfluorohexyl iodide (355-43-1) → 2-tridecafluorohexyl-1,1-dimethoxyethane (142502-76-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 5 percent Spectr_. / Zn / CH₂Cl₂ / 5 h / 25 °C

2: 95 percent Spectr_. / 5 h / 60 °C

With zinc; In dichloromethane;

DOI:10.1016/S0040-4039(00)92222-6

Reference yield:

2-F-Hexyl-2-brom-aethen (51249-64-0) → 2-tridecafluorohexyl-1,1-dimethoxyethane (142502-76-9)

Guidance literature:

Multi-step reaction with 2 steps

1: KOH / 1 h / Heating

2: 87 percent / p-toluenesulfonic acid / CH₂Cl₂ / 24 h / 40 °C

With potassium hydroxide; toluene-4-sulfonic acid; In dichloromethane;

DOI:10.1016/j.jfluchem.2004.07.001

upstream raw materials:

methanol

Acetic acid 3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-1-iodo-octyl ester

2-F-Hexyl-2-brom-aethen

n-perfluorohexyl iodide

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 142502-76-9 2-(PERFLUORO-N-HEXYL)ACETALDEHYDE DIMETHYL ACETAL

Send

Send

Metric Ton KG G Pound L ML

Send

Send