alpha-D-erythro-Pentofuranoside,ethyl2-deoxy-3-O-(1-methylethyl)-(9CI)

Base Information

• Chemical Name: alpha-D-erythro-Pentofuranoside,ethyl2-deoxy-3-O-(1-methylethyl)-(9CI)
• CAS No.: 146764-52-5
• Molecular Formula: C₁₀H₂₀O₄
• Molecular Weight: 204.266
• Mol file: 146764-52-5.mol

Synonyms:alpha-D-erythro-Pentofuranoside,ethyl2-deoxy-3-O-(1-methylethyl)-(9CI)

Chemical Property of alpha-D-erythro-Pentofuranoside,ethyl2-deoxy-3-O-(1-methylethyl)-(9CI)

Chemical Property:

• Boiling Point: 283.8±40.0 °C(Predicted)
• PKA: 14.44±0.10(Predicted)
• Density: 1.05±0.1 g/cm3(Predicted)

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

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Technology Process of alpha-D-erythro-Pentofuranoside,ethyl2-deoxy-3-O-(1-methylethyl)-(9CI)

There total 2 articles about alpha-D-erythro-Pentofuranoside,ethyl2-deoxy-3-O-(1-methylethyl)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,4-Anhydro-2-deoxy-D-threo-pentose diethyl acetal (138665-68-6) → Ethyl 3-fluoro-2,3-dideoxy-D-riboside (146764-50-3,146764-51-4) + 3-fluoro-2,3-dideoxy-D-erythro-pentose diethyl acetal (146764-48-9) + ((2R,3S)-5-Ethoxy-3-isopropoxy-tetrahydro-furan-2-yl)-methanol (146764-52-5,146764-53-6) + (2R,3S)-5,5-Diethoxy-3-isopropoxy-pentane-1,2-diol (146764-49-0)

Guidance literature:

With titanium(IV) isopropylate; benzoyl fluoride; In benzene; at 80 ℃; for 0.1h; Yield given. Yields of byproduct given;

DOI:10.1016/S0040-4039(00)60842-0

Reference yield:

3,4-Anhydro-2-deoxy-D-threo-pentose diethyl acetal (138665-68-6) + titanium(IV)isopropoxide (546-68-9) → Ethyl 3-fluoro-2,3-dideoxy-D-riboside (146764-50-3,146764-51-4) + 3-fluoro-2,3-dideoxy-D-erythro-pentose diethyl acetal (146764-48-9) + ((2R,3S)-5-Ethoxy-3-isopropoxy-tetrahydro-furan-2-yl)-methanol (146764-52-5,146764-53-6) + (2R,3S)-5,5-Diethoxy-3-isopropoxy-pentane-1,2-diol (146764-49-0)

Guidance literature:

With benzoyl fluoride; Yield given. Multistep reaction. Yields of byproduct given; 2) hexane, 0.5 h, 69 deg C;

DOI:10.1016/S0040-4039(00)60842-0

upstream raw materials:

3,4-Anhydro-2-deoxy-D-threo-pentose diethyl acetal

titanium(IV)isopropoxide

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