Ethyl 3-bromo-4-methylbenzoate

Base Information

Chemical Name:Ethyl 3-bromo-4-methylbenzoate
CAS No.:147962-81-0
Molecular Formula:C10H11 Br O2
Molecular Weight:243.1
Hs Code.:2916399090
DSSTox Substance ID:DTXSID60565862
Nikkaji Number:J2.647.658E
Wikidata:Q72473264
Mol file:147962-81-0.mol

Synonyms:Ethyl 3-bromo-4-methylbenzoate;147962-81-0;Benzoic acid, 3-bromo-4-methyl-, ethyl ester;MFCD11042852;3-Bromo-4-methyl-benzoic acid ethyl ester;Ethyl3-bromo-4-methylbenzoate;SCHEMBL670944;DTXSID60565862;ILZQYNXOOLMOGA-UHFFFAOYSA-N;XFA96281;AKOS015843454;FS-4502;MB09092;SY291399;CS-0151794;D70717;A808715

Suppliers and Price of Ethyl 3-bromo-4-methylbenzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
Ethyl3-bromo-4-methylbenzoate
25g
$ 75.00

Rieke Metals
3-Bromo-4-methyl-benzoicacidethylester
1g
$ 661.00

Crysdot
Ethyl3-bromo-4-methylbenzoate 95+%
5g
$ 628.00

AOBChem
Ethyl3-bromo-4-methylbenzoate 97%
5g
$ 59.00

American Custom Chemicals Corporation
ETHYL-3-BROMO-4-METHYLBENZOATE 95.00%
5MG
$ 500.85

Ambeed
Ethyl3-bromo-4-methylbenzoate 98+%
100g
$ 42.00

Ambeed
Ethyl3-bromo-4-methylbenzoate 98+%
25g
$ 42.00

Ambeed
Ethyl3-bromo-4-methylbenzoate 98+%
1g
$ 5.00

Ambeed
Ethyl3-bromo-4-methylbenzoate 98+%
5g
$ 5.00

Alichem
Ethyl3-bromo-4-methylbenzoate
1g
$ 163.20

Total 8 raw suppliers

Chemical Property of Ethyl 3-bromo-4-methylbenzoate

Chemical Property:

Vapor Pressure:0.00316mmHg at 25°C
Refractive Index:1.538
Boiling Point:283.5°Cat760mmHg
Flash Point:125.2°C
PSA：26.30000
Density:1.378g/cm³
LogP:2.93420
Storage Temp.:Sealed in dry,Room Temperature
XLogP3:3.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:241.99424
Heavy Atom Count:13
Complexity:182

Purity/Quality:

97% ^*data from raw suppliers

Ethyl3-bromo-4-methylbenzoate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)C1=CC(=C(C=C1)C)Br

Technology Process of Ethyl 3-bromo-4-methylbenzoate

There total 7 articles about Ethyl 3-bromo-4-methylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 64-17-5
ethanol

: 7697-26-9
3-bromo-4-methylbenzoic acid

: 147962-81-0
ethyl 3-bromo-4-methylbenzoate

Guidance literature:: With sulfuric acid; at 75 ℃; for 5h;

Reference yield: 78.0%

: 7697-26-9
3-bromo-4-methylbenzoic acid

: 75-03-6
ethyl iodide

: 147962-81-0
ethyl 3-bromo-4-methylbenzoate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 168h;
DOI:10.1016/j.bmc.2011.03.003

Reference yield:

: 41191-92-8
3-amino-4-methylbenzoic acid ethyl ester

: 147962-81-0
ethyl 3-bromo-4-methylbenzoate

Guidance literature:: With hydrogen bromide; copper(I) bromide; sodium nitrite; Yield given. Multistep reaction; 1.) -5 deg C, 5 min, 2.) 70 deg C, 1 h;
DOI:10.1021/ja00061a019