2,3-DIBBROME-1-PROPANESULFONIC ACID SODIUM SALT

Base Information

• Chemical Name: 2,3-DIBBROME-1-PROPANESULFONIC ACID SODIUM SALT
• CAS No.: 51116-03-1
• Molecular Formula: C3H5Br2O3S.Na
• Molecular Weight: 303.935
• Hs Code.: 2904909090
• Mol file: 51116-03-1.mol

Synonyms:2,3-DIBBROME-1-PROPANESULFONIC ACID SODIUM SALT

Chemical Property of 2,3-DIBBROME-1-PROPANESULFONIC ACID SODIUM SALT

Chemical Property:

• PSA: 65.58000
• LogP: 1.77080
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

98%,99%, ^*data from raw suppliers

Sodium 2,3-dibromopropane-1-sulfonate 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,3-DIBBROME-1-PROPANESULFONIC ACID SODIUM SALT

There total 2 articles about 2,3-DIBBROME-1-PROPANESULFONIC ACID SODIUM SALT which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

sodium prop-2-ene-1-sulfonate (2495-39-8) → sodium 2,3-dibromopropane-1-sulfonate (51116-03-1)

Guidance literature:

With bromine; In water; at 20 ℃; for 2h;

DOI:10.1055/s-2003-40201 DOI:10.1002/jhet.5570400616

Reference yield:

→ sodium 2,3-dibromopropane-1-sulfonate (51116-03-1)

Guidance literature:

With bromine; acetic acid;

DOI:10.1039/jr9550001302

Reference yield:

lead acetate (301-04-2) + sodium 2,3-dibromopropane-1-sulfonate (51116-03-1) → unithiol (4076-02-2)

Guidance literature:

sodium 2,3-dibromopropane-1-sulfonate; With sodium ethanolate; In ethanol; at 23 - 25 ℃; for 1.5h; under 2250.23 - 3750.38 Torr;

lead acetate; In water; at 50 - 55 ℃; for 1h; Reagent/catalyst; Temperature; Further stages;

upstream raw materials:

sodium prop-2-ene-1-sulfonate

Downstream raw materials:

2-bromopropane-1,3-sultone

unithiol

Refernces

• 1、 -. "A kind of improved 2, 3 - dimercapto method for the synthesis of the sodium". Paragraph 0032; 0035; 0036; 0037. . Retrieved 2018/11/03.
• 2、 Tian, Li,Xu, Guo-Yan,Ye, Yong,Liu, Lun-Zu. "1,3-Dipolar Cycloaddition Reactions of Nitrile Oxides to Prop-1-ene-1,3-sultone". . p. 1071 - 1074. Retrieved 2007/10/03.