o-Diphenetidine

Base Information

• Chemical Name: o-Diphenetidine
• CAS No.: 6264-77-3
• Molecular Formula: C16H20N2O2
• Molecular Weight: 272.347
• Mol file: 6264-77-3.mol

Synonyms:o-Diphenetidine

Chemical Property of o-Diphenetidine

Chemical Property:

• PSA: 70.50000
• LogP: 4.47780

Purity/Quality:

98%min ^*data from raw suppliers

3,3'-Diethoxybiphenyl-4,4'-diamine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of o-Diphenetidine

There total 5 articles about o-Diphenetidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.63%

2,2'-diethoxyhydrazobenzene (1033-71-2) → 4,4'-diamino-3,3'-diethoxybiphenyl (6264-77-3)

Guidance literature:

2,2'-diethoxyhydrazobenzene; With hydrogenchloride; In water; at 30 - 90 ℃; for 2h;

With water; sodium hydroxide; pH=9 - 10;

Reference yield:

1-ethoxy-2-nitrobenzene (610-67-3) → 4,4'-diamino-3,3'-diethoxybiphenyl (6264-77-3)

Guidance literature:

Multi-step reaction with 2 steps

1: zinc; aq.-ethanolic NaOH-solution

2: hydrogen chloride; ethanol

With hydrogenchloride; sodium hydroxide; ethanol; zinc;

DOI:10.1039/jr9330000984

Reference yield:

2,2'-diethoxyazobenzene (613-43-4) → 4,4'-diamino-3,3'-diethoxybiphenyl (6264-77-3)

Guidance literature:

Multi-step reaction with 2 steps

1: alcoholic ammonium sulfide

2: concentrated hydrochloric acid

With hydrogenchloride; ammonium sulfide;

upstream raw materials:

2,2'-diethoxyhydrazobenzene

hydrogenchloride

1-ethoxy-2-nitrobenzene

2,2'-diethoxyazobenzene

Downstream raw materials:

3,3'-dihydroxybenzidine

N',N'''-diphenyl-N,N''-(3,3'-diethoxy-biphenyl-4,4'-diyl)-di-urea