ethyl 2,4-dimethyl-3-furoate

Base Information

• Chemical Name: ethyl 2,4-dimethyl-3-furoate
• CAS No.: 6148-33-0
• Molecular Formula: C9H12O3
• Molecular Weight: 168.19
• Hs Code.: 2932190090
• Mol file: 6148-33-0.mol

Synonyms:ethyl 2,4-dimethyl-3-furoate

Chemical Property of ethyl 2,4-dimethyl-3-furoate

Chemical Property:

• PSA: 39.44000
• LogP: 2.07310

Purity/Quality:

98%Min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ethyl 2,4-dimethyl-3-furoate

There total 28 articles about ethyl 2,4-dimethyl-3-furoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

ethyl 2-acetyl-4-bromopent-4-enoate (90674-91-2) → ethyl 2,4-dimethylfuran-3-carboxylate (6148-33-0)

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 1h;

DOI:10.1039/c5ra14273c

Reference yield: 62.0%

3-acetoxy-2-chloroprop-1-ene (692-72-8) + sodium ethyl acetoacetate → ethyl 2,4-dimethylfuran-3-carboxylate (6148-33-0)

Guidance literature:

With ethylenebis(triphenylphosphine)platinum⁽⁰⁾; In tetrahydrofuran; at 80 ℃; for 2h;

DOI:10.1021/jo990845x

Reference yield: 62.0%

1,2,3-tribromopropane (96-11-7) + ethyl acetoacetate (141-97-9) → ethyl 2,4-dimethylfuran-3-carboxylate (6148-33-0)

Guidance literature:

With potassium carbonate; In dimethyl sulfoxide; Heating;

DOI:10.1007/BF00503618

upstream raw materials:

ethanol

ethyl acetoacetate

(E)-3-Ureido-but-2-enoic acid ethyl ester

hydroxy-2-propanone

Downstream raw materials:

2-(2,4-Dimethyl-furan-3-ylmethyl)-5-methyl-benzene-1,3-diol

4-(2,4-Dimethyl-furan-3-ylmethyl)-5-methyl-benzene-1,3-diol

2,4-dimethyl-3-furylmethyl benzoate

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