ethyl phenyl(prop-2-en-1-yl)carbamate

Base Information Edit

Chemical Name:ethyl phenyl(prop-2-en-1-yl)carbamate
CAS No.:7451-54-9
Molecular Formula:C12H15 N O2
Molecular Weight:205.257
Hs Code.:
Mol file:7451-54-9.mol

Synonyms:Carbanilicacid, N-allyl-, ethyl ester (6CI,7CI,8CI); Ethyl N-allyl-N-phenylcarbamate;Ethyl N-allylcarbanilate; NSC 60567

Suppliers and Price of ethyl phenyl(prop-2-en-1-yl)carbamate

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 4 raw suppliers

Chemical Property of ethyl phenyl(prop-2-en-1-yl)carbamate Edit

Chemical Property:

Vapor Pressure:0.00313mmHg at 25°C
Boiling Point:283.6°C at 760 mmHg
Flash Point:125.3°C
Density:1.068g/cm³

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of ethyl phenyl(prop-2-en-1-yl)carbamate

There total 3 articles about ethyl phenyl(prop-2-en-1-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.9%

: 101-99-5
N-carboethoxyaniline

: 106-95-6
allyl bromide

: 7451-54-9
ethyl allyl(phenyl)carbamate

Guidance literature:: N-carboethoxyaniline; With sodium hydride; In tetrahydrofuran; at 20 ℃; for 0.5h; Inert atmosphere;

allyl bromide; With tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.tet.2013.01.052

Reference yield:

: 62-53-3
aniline

: 7451-54-9
ethyl allyl(phenyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

2.1: sodium hydride / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

2.2: 1 h / 20 °C / Inert atmosphere

With sodium hydride; potassium carbonate; In tetrahydrofuran;
DOI:10.1016/j.tet.2013.01.052