BENZOYL-DL-A-ALANINE ETHYL ESTER

Base Information

• Chemical Name: BENZOYL-DL-A-ALANINE ETHYL ESTER
• CAS No.: 5446-46-8
• Molecular Formula: C12H15NO3
• Molecular Weight: 221.256
• Hs Code.: 2924299090
• Mol file: 5446-46-8.mol

Synonyms:BENZOYL-DL-A-ALANINE ETHYL ESTER

Chemical Property of BENZOYL-DL-A-ALANINE ETHYL ESTER

Chemical Property:

• Vapor Pressure: 2.09E-06mmHg at 25°C
• Refractive Index: 1.514
• Boiling Point: 393.7°C at 760 mmHg
• Flash Point: 191.9°C
• PSA: 55.40000
• Density: 1.108g/cm³
• LogP: 1.75890

Purity/Quality:

99% ^*data from raw suppliers

BENZOYL-DL-A-ALANINE ETHYL ESTER 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of BENZOYL-DL-A-ALANINE ETHYL ESTER

There total 18 articles about BENZOYL-DL-A-ALANINE ETHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

AlaOEt (17344-99-9) + benzoyl chloride (98-88-4) → ethyl 2-(benzoylamino)propanoate (5446-46-8)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃;

DOI:10.1039/c8md00139a

Reference yield: 75.0%

ethyl 2-azido-2-methyl-3-oxo-3-phenylpropanoate (235096-50-1) → ethyl 2-(benzoylamino)propanoate (5446-46-8) + ethyl 2-benzoylpropionate (10488-87-6)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; Heating;

DOI:10.1021/jo990837g

Reference yield: 73.0%

ethyl 2-azidopropanoate (71754-74-0) + benzoic acid (65-85-0,8013-63-6) → ethyl 2-(benzoylamino)propanoate (5446-46-8)

Guidance literature:

With tributylphosphine; In toluene; Mechanism; Heating; var. reagents, solv., temp., other azides and acids;

DOI:10.1021/jo00214a048

upstream raw materials:

2-phenyl-4-methyl-4H-oxazolin-5-one

ethanol

N-Benzoylalanine

ethyl (Z)-3-benzoyloxy-2-benzamidoacrylate

Downstream raw materials:

L-Alanine, N-benzoyl-, ethyl ester

N-benzoyl-D-alanine ethyl ester

N-benzoyl-N'-(N-benzoyl-alanyl)-hydrazine

N,N'-bis-(N-benzoyl-alanyl)-hydrazine