(1S,2S)-N,N,N''N''-TETRAMETHYL-1,2-CYCLOHEXANEDIAMINE

Base Information

• Chemical Name: (1S,2S)-N,N,N''N''-TETRAMETHYL-1,2-CYCLOHEXANEDIAMINE
• CAS No.: 53152-68-4
• Molecular Formula: C10H22N2
• Molecular Weight: 170.298
• Hs Code.: 2921300090
• Mol file: 53152-68-4.mol

Synonyms:(1S,2S)-N,N,N''N''-TETRAMETHYL-1,2-CYCLOHEXANEDIAMINE

Chemical Property of (1S,2S)-N,N,N''N''-TETRAMETHYL-1,2-CYCLOHEXANEDIAMINE

Chemical Property:

• Boiling Point: 216.8±8.0 °C(Predicted)
• PKA: 10.81±0.70(Predicted)
• PSA: 6.48000
• Density: 0.89±0.1 g/cm3(Predicted)
• LogP: 1.42080
• Storage Temp.: under inert gas (nitrogen or Argon) at 2–8 °C

Purity/Quality:

97% ^*data from raw suppliers

(1S,2S)-N1,N1,N2,N2-Tetramethylcyclohexane-1,2-diamine 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (1S,2S)-N,N,N''N''-TETRAMETHYL-1,2-CYCLOHEXANEDIAMINE

There total 27 articles about (1S,2S)-N,N,N''N''-TETRAMETHYL-1,2-CYCLOHEXANEDIAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + (1R,2R)-1,2-diaminocyclohexane tartrate (32044-22-7,39961-95-0) → (1R,2R)-bis(dimethylamino)cyclohexane (38383-49-2,43148-65-8,46026-77-1,53100-04-2,53152-68-4,53152-69-5)

Guidance literature:

With formic acid; Heating;

DOI:10.1016/j.tetlet.2003.09.171

Reference yield: 54.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + (1R,2R)-1,2-diaminocyclohexane (20439-47-8) → (1R,2R)-bis(dimethylamino)cyclohexane (38383-49-2,43148-65-8,46026-77-1,53100-04-2,53152-68-4,53152-69-5)

Guidance literature:

With sodium cyanoborohydride; In acetonitrile; at 0 - 25 ℃; for 3h; Inert atmosphere;

DOI:10.1021/ja5109084

Reference yield: 47.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + trans-1,2-Diaminocyclohexane (1121-22-8,1436-59-5,20439-47-8,21436-03-3,41013-43-8,694-83-7) → trans-N,N,N′,N′-tetramethylcyclohexane-1,2-diamine (1121-22-8,38383-49-2,43148-65-8,46026-77-1,53100-04-2,53152-68-4,53152-69-5)

Guidance literature:

With formic acid; In water; at 0 - 80 ℃;

DOI:10.1021/ja970029b

upstream raw materials:

formaldehyd

(S,S)-1,2-diaminocyclohexane

formic acid

(1R,2R)-N,N-dimethylcyclohexane-1,2-diamine

Downstream raw materials:

(R,R)-C₆H₁₀(NMe₂)(NMeCH₂SiPh₂Me)

(1R,2R)-N₁-[{(tert-butylamino)dimethylsilyl}methyl]-N₁,N₂,N₂-trimethylcyclohexane-1,2-diamine

diethyl ether

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