o-Butoxybromobenzene

Base Information

• Chemical Name: o-Butoxybromobenzene
• CAS No.: 54514-30-6
• Molecular Formula: C10H13BrO
• Molecular Weight: 229.117
• Hs Code.: 2909309090
• Mol file: 54514-30-6.mol

Synonyms:o-Butoxybromobenzene

Chemical Property of o-Butoxybromobenzene

Chemical Property:

• PSA: 9.23000
• LogP: 3.62800

Purity/Quality:

99% ^*data from raw suppliers

1-Bromo-2-butoxybenzene ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of o-Butoxybromobenzene

There total 2 articles about o-Butoxybromobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

1-iodo-butane (542-69-8) + 2-hydroxybromobenzene (95-56-7) → 1-bromo-2-n-butoxybenzene (54514-30-6)

Guidance literature:

With sodium hydroxide; In water; N,N-dimethyl-formamide; at 20 ℃; for 4h;

DOI:10.1016/j.tet.2012.03.060

Reference yield:

1-bromo-butane (109-65-9) + 2-hydroxybromobenzene (95-56-7) → 1-bromo-2-n-butoxybenzene (54514-30-6)

Guidance literature:

With potassium hydroxide;

Reference yield: 76.0%

tris(dibenzylideacetone)dipalladium + 1-bromo-2-n-butoxybenzene (54514-30-6) + 1-(1,1-dimethylethyl)-piperazine (38216-72-7) → 4-phenyl-1-piperazine (92-54-6)

Guidance literature:

With sodium t-butanolate; In toluene;

upstream raw materials:

1-bromo-butane

2-hydroxybromobenzene

1-iodo-butane

Downstream raw materials:

4-phenyl-1-piperazine

4-(2-n-butoxyphenyl)-1,2,3,3a,4,8b-hexahydrocyclopenta[b]indole

4-(2-n-butoxyphenyl)-1,2,3,3a,4,8b-hexahydrocyclopenta[b]indole-7-carbaldehyde

C₂₆H₂₈ClNO₄S

Refernces