1H-Pyrrolo[1,2-a]benzimidazole,8-chloro-2,3-dihydro-(7CI,9CI)

Base Information

Chemical Name:1H-Pyrrolo[1,2-a]benzimidazole,8-chloro-2,3-dihydro-(7CI,9CI)
CAS No.:59506-73-9
Molecular Formula:C10H9ClN2
Molecular Weight:192.64
Hs Code.:
Mol file:59506-73-9.mol

Synonyms:1H-Pyrrolo[1,2-a]benzimidazole,8-chloro-2,3-dihydro-(7CI,9CI)

Suppliers and Price of 1H-Pyrrolo[1,2-a]benzimidazole,8-chloro-2,3-dihydro-(7CI,9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of 1H-Pyrrolo[1,2-a]benzimidazole,8-chloro-2,3-dihydro-(7CI,9CI)

Chemical Property:

PSA：17.82000
LogP:2.63590

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1H-Pyrrolo[1,2-a]benzimidazole,8-chloro-2,3-dihydro-(7CI,9CI)

There total 3 articles about 1H-Pyrrolo[1,2-a]benzimidazole,8-chloro-2,3-dihydro-(7CI,9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 123-75-1
pyrrolidine

: 932-78-5
1-chloro-3-nitrosobenzene

: 10252-95-6
6-Chlor-2,3-dihydro-1H-pyrrolo<1,2-a>benzimidazol

: 59506-73-9
8-chloro-2,3-dihydro-1H-benzo[d]pyrrolo[1,2-a]imidazole

Guidance literature:: With 2,4 dichlorobenzoic acid; In toluene; at 20 - 110 ℃; for 8.33h; Inert atmosphere;
DOI:10.1021/acs.orglett.7b00832

Reference yield:

: 108-42-9
3-chloro-aniline

: 10252-95-6
6-Chlor-2,3-dihydro-1H-pyrrolo<1,2-a>benzimidazol

: 59506-73-9
8-chloro-2,3-dihydro-1H-benzo[d]pyrrolo[1,2-a]imidazole

Guidance literature:: Multi-step reaction with 2 steps

1: Oxone / dichloromethane; water / 4 h / 20 °C / Inert atmosphere

2: 2,4 dichlorobenzoic acid / toluene / 8.33 h / 20 - 110 °C / Inert atmosphere

With Oxone; 2,4 dichlorobenzoic acid; In dichloromethane; water; toluene;
DOI:10.1021/acs.orglett.7b00832