ETHYL-FURAN-2-YLMETHYL-AMINE

Base Information

• Chemical Name: ETHYL-FURAN-2-YLMETHYL-AMINE
• CAS No.: 14496-33-4
• Molecular Formula: C7H11 N O
• Molecular Weight: 125.17
• Hs Code.: 2932190090
• Mol file: 14496-33-4.mol

Synonyms:Furfurylamine,N-ethyl- (8CI); N-Ethylfurfurylamine

Chemical Property of ETHYL-FURAN-2-YLMETHYL-AMINE

Chemical Property:

• Vapor Pressure: 2.88mmHg at 25°C
• Refractive Index: 1.469
• Boiling Point: 156.5°C at 760 mmHg
• Flash Point: 48.5°C
• PSA: 25.17000
• Density: 0.96g/cm³
• LogP: 1.78000
• Storage Temp.: 2-8°C(protect from light)

Purity/Quality:

98%min ^*data from raw suppliers

N-(2-Furylmethyl)ethanamine ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi,Xn
• Statements: 22

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ETHYL-FURAN-2-YLMETHYL-AMINE

There total 10 articles about ETHYL-FURAN-2-YLMETHYL-AMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

(2-furyl)methyl alcohol (98-00-0,25212-86-6,93793-62-5) + acetonitrile (75-05-8,26809-02-9) → 1-ethyl-piperidine (766-09-6) + ethyl(furan-2-ylmethyl)amine (14496-33-4)

Guidance literature:

With hydrogen; magnesium oxide; copper; at 230 ℃; under 11400 Torr;

DOI:10.1007/BF00475557

Reference yield: 50.0%

(2-furyl)methyl alcohol (98-00-0,25212-86-6,93793-62-5) + acetonitrile (75-05-8,26809-02-9) → 1-ethyl-piperidine (766-09-6) + ethyl(furan-2-ylmethyl)amine (14496-33-4)

Guidance literature:

With hydrogen; magnesium oxide; copper; at 230 ℃; under 11400 Torr; Mechanism; Product distribution; other catalysts; other temperature; other pressure;

DOI:10.1007/BF00475557

Reference yield:

ethanol (64-17-5) + 3-ethylamino-3-[2]furyl-2-nitro-propionic acid ethyl ester (874005-46-6) → ethyl(furan-2-ylmethyl)amine (14496-33-4) + GlyOEt*HCl (459-73-4)

Guidance literature:

Hydrogenation;

upstream raw materials:

2-bromomethylfuran

N-ethylfuran-2-carboxamide

ethyl-furfurylidene-amine

3-ethylamino-3-[2]furyl-2-nitro-propionic acid ethyl ester

Downstream raw materials:

N-ethyl-N-(furan-2-ylmethyl)-2-(p-tolyloxy)acetamide

C₁₇H₂₁N₃O₃

6-(Ethyl-furan-2-ylmethyl-amino)-1,3-dimethyl-5-(phenyl-hydrazonomethyl)-1H-pyrimidine-2,4-dione

Refernces

• 1、 Kozintsev, S. I.,Basalaeva, L. I.,Gladkikh, L. V.,Kozlov, N. S.. "Catalytic Hydroamination of Furfuryl and Tetrahydrofurfuryl Alcohols with Nitriles". . p. 19 - 21. Retrieved 1988.