2,6-dioxopiperidine-4-carboxylic acid

Base Information

• Chemical Name: 2,6-dioxopiperidine-4-carboxylic acid
• CAS No.: 6973-55-3
• Molecular Formula: C6H7 N O4
• Molecular Weight: 157.126
• Hs Code.: 2925190090
• Mol file: 6973-55-3.mol

Synonyms:Isonipecoticacid, 2,6-dioxo- (6CI); 2,6-Dioxopiperidine-4-carboxylic acid; NSC 40229

Chemical Property of 2,6-dioxopiperidine-4-carboxylic acid

Chemical Property:

• Vapor Pressure: 5.9E-10mmHg at 25°C
• Boiling Point: 465.5°Cat760mmHg
• Flash Point: 235.3°C
• PSA: 83.47000
• Density: 1.458g/cm³
• LogP: -0.54740

Purity/Quality:

97% ^*data from raw suppliers

2,6-Dioxo-4-piperidinecarboxylicAcid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 2,6-Dioxo-4-piperidinecarboxylic Acid is used as a reagent in the synthesis of thiazoline analogs of epiderstatin as new inhibitors of cell cycle of tsFT-210 cells.

Technology Process of 2,6-dioxopiperidine-4-carboxylic acid

There total 4 articles about 2,6-dioxopiperidine-4-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

4-phenylpiperidine-2,6-dione (14149-31-6) → 2,6-dioxopiperidine-4-carboxylic acid (6973-55-3)

Guidance literature:

With ruthenium trichloride; sodium periodate; for 36h; Ambient temperature;

DOI:10.7164/antibiotics.48.1179

Reference yield:

citrazinic acid (99-11-6) → 2,6-dioxopiperidine-4-carboxylic acid (6973-55-3)

Guidance literature:

With palladium on activated charcoal; ethanol; at 50 ℃; under 2574.3 Torr; Hydrogenation;

Reference yield:

3-phenylglutaric acid (4165-96-2) → 2,6-dioxopiperidine-4-carboxylic acid (6973-55-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 97 percent / urea / 2 h / 150 °C

2: 85 percent / aq. NaIO₄, RuCl₃ / 36 h / Ambient temperature

With ruthenium trichloride; sodium periodate; urea;

DOI:10.7164/antibiotics.48.1179

upstream raw materials:

citrazinic acid

4-phenylpiperidine-2,6-dione

3-phenylglutaric acid

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