4-(6-Methoxypyridin-2-yl)benzaldehyde

Base Information

• Chemical Name: 4-(6-Methoxypyridin-2-yl)benzaldehyde
• CAS No.: 618092-16-3
• Molecular Formula: C13H11NO2
• Molecular Weight: 213.236
• European Community (EC) Number: 651-586-5
• Mol file: 618092-16-3.mol

Synonyms:4-(6-methoxypyridin-2-yl)benzaldehyde;SCHEMBL610482;OQYLQLAVBZSSDL-UHFFFAOYSA-N;MFCD05150363;AKOS024015197;4-(6-methoxy-pyridine-2-yl)-benzaldehyde;CS-0195593;4-(6-METHOXY-2-PYRIDINYL)BENZALDEHYDE

Chemical Property of 4-(6-Methoxypyridin-2-yl)benzaldehyde

Chemical Property:

• XLogP3: 2.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 3
• Exact Mass: 213.078978594
• Heavy Atom Count: 16
• Complexity: 224

Purity/Quality:

98% ^*data from raw suppliers

4-(6-Methoxypyridin-2-yl)benzaldehyde 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=CC=CC(=N1)C2=CC=C(C=C2)C=O

Technology Process of 4-(6-Methoxypyridin-2-yl)benzaldehyde

There total 1 articles about 4-(6-Methoxypyridin-2-yl)benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

6-methoxy-2-pyridylboronic acid N-methyliminodiacetic acid ester (1227700-45-9) + 4-bromo-benzaldehyde (1122-91-4) → 4-(6-methoxypyridin-2-yl)benzaldehyde (618092-16-3)

Guidance literature:

With potassium carbonate; In ethanol; water; for 8h; Reflux; Green chemistry;

DOI:10.1039/c4ra03586k

Reference yield: 91.0%

4-(6-methoxypyridin-2-yl)benzaldehyde (618092-16-3) + 2-naphthohydrazide (39627-84-4) → (E)-N'-(4-(6-methoxypyridin-2-yl)benzylidene)-2-naphthohydrazide

Guidance literature:

With hydrogenchloride; In ethanol; water; at 20 ℃; for 3h;

DOI:10.1111/cbdd.13085

Reference yield: 90.0%

4-(6-methoxypyridin-2-yl)benzaldehyde (618092-16-3) + (trifluoromethyl)trimethylsilane (81290-20-2) → 1-[4-(6-methoxypyridin-2-yl)phenyl]-2,2,2-trifluoroethanol (1033805-85-4)

Guidance literature:

4-(6-methoxypyridin-2-yl)benzaldehyde; (trifluoromethyl)trimethylsilane; With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 - 20 ℃; for 4h;

With hydrogenchloride; water; In tetrahydrofuran;

upstream raw materials:

6-methoxy-2-pyridylboronic acid N-methyliminodiacetic acid ester

4-bromo-benzaldehyde

Downstream raw materials:

1-[4-(6-methoxypyridin-2-yl)phenyl]-2,2,2-trifluoroethanol

(S)-2-amino-3-[4-(2-amino-6-{2,2,2-trifluoro-1-[4-(6-methoxy-pyridin-2-yl)-phenyl]-ethoxy}-pyrimidin-4-yl)-phenyl]-propionic acid

(S)-3-[4-(2-amino-6-{2,2,2-trifluoro-1-[4-(6-methoxypyridin-2-yl)phenyl]ethoxy}pyrimidin-4-yl)phenyl]-2-tert-butoxycarbonylaminopropionic acid

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