3-Pyridazinecarboxylicacid,6-methyl-,ethylester(9CI)

Base Information

• Chemical Name: 3-Pyridazinecarboxylicacid,6-methyl-,ethylester(9CI)
• CAS No.: 64210-57-7
• Molecular Formula: C₈H₁₀N₂O₂
• Molecular Weight: 166.18
• Hs Code.: 2933990090
• Mol file: 64210-57-7.mol

Synonyms:3-Pyridazinecarboxylicacid,6-methyl-,ethylester(9CI)

Chemical Property of 3-Pyridazinecarboxylicacid,6-methyl-,ethylester(9CI)

Chemical Property:

• PSA: 52.08000
• LogP: 0.96170
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

Ethyl6-methylpyridazine-3-carboxylate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-Pyridazinecarboxylicacid,6-methyl-,ethylester(9CI)

There total 3 articles about 3-Pyridazinecarboxylicacid,6-methyl-,ethylester(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

2-acetyl-5-oxohexanoic acid ethyl ester (35490-05-2) + hydrazine hydrate (7803-57-8,79785-97-0) → ethyl 6-methylpyridazine-3-carboxylate (64210-57-7)

Guidance literature:

2-acetyl-5-oxohexanoic acid ethyl ester; With manganese(III) triacetate dihydrate; acetic acid; cobalt(II) chloride; at 25 ℃; for 3h;

hydrazine hydrate; at 60 ℃; for 0.5h;

Reference yield: 24.0%

2-acetyl-5-oxohexanoic acid ethyl ester (35490-05-2) → ethyl 6-methylpyridazine-3-carboxylate (64210-57-7)

Guidance literature:

2-acetyl-5-oxohexanoic acid ethyl ester; With manganese(III) triacetate dihydrate; acetic acid; cobalt(II) chloride; at 25 ℃; for 3h;

With hydrazine hydrate; at 60 ℃; for 0.5h;

DOI:10.1039/c4ob02441a

Reference yield:

sodium carbonate (497-19-8) + 6-methyl-3-pyridazinecarboxylic acid (64210-60-2) + 1,2-dichloro-ethane (107-06-2,52399-93-6) → ethyl 6-methylpyridazine-3-carboxylate (64210-57-7)

Guidance literature:

With methanesulfonic acid; In ethanol; water;

upstream raw materials:

sodium carbonate

6-methyl-3-pyridazinecarboxylic acid

1,2-dichloro-ethane

2-acetyl-5-oxohexanoic acid ethyl ester

Downstream raw materials:

(6-methylpyridazin-3-yl)methanol

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