(PPh₂C₅H₄)Fe(C₅H₄CHCHCOC₅H₄N)

Base Information

Chemical Name:(PPh₂C₅H₄)Fe(C₅H₄CHCHCOC₅H₄N)
CAS No.:1246383-83-4
Molecular Formula:C₃₀H₂₄FeNOP
Molecular Weight:501.347
Hs Code.:

(PPh<sub>2</sub>C<sub>5</sub>H<sub>4</sub>)Fe(C<sub>5</sub>H<sub>4</sub>CHCHCOC<sub>5</sub>H<sub>4</sub>N)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (PPh₂C₅H₄)Fe(C₅H₄CHCHCOC₅H₄N)

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Technology Process of (PPh₂C₅H₄)Fe(C₅H₄CHCHCOC₅H₄N)

There total 1 articles about (PPh₂C₅H₄)Fe(C₅H₄CHCHCOC₅H₄N) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1122-62-9
2-acetylpyridine

: 124944-40-7
1′-(diphenylphosphino)ferrocene-1-carbaldehyde

: 1246383-83-4
(PPh₂C₅H₄)Fe(C₅H₄CHCHCOC₅H₄N)

Guidance literature:: With NaOH; In ethanol; dichloromethane; under Ar, using Schlenk technique; Fc complex dissolved in CH2Cl2 and EtOH, acetylpyridine added to mixt.; stirred for 5 min; NaOH soln. droppedinto mixt., stirred for 2.5 h at 25°C; react. mixt. evapd., water added; extd. twice with CH2Cl2; org. phases combined, dried with MgSO4; volatiles removed in vac.; purified by columnchromy. on silica gel using EtOAc; volatiles removed under reduced pres sure; elem. anal.;
DOI:10.1002/ejic.201000365

Reference yield: 90.0%

: 12107-56-1
dichloro(1,5-cyclooctadiene)palladium(II)

: 75-09-2
dichloromethane

: 1246383-83-4
(PPh₂C₅H₄)Fe(C₅H₄CHCHCOC₅H₄N)

: Cl₂Pd(C₅H₄P(C₆H₅)2)Fe(C₅H₄CHCHCOC₅H₄N)*0.5CH₂Cl₂*H₂O

Guidance literature:: In dichloromethane; under Ar, using Schlenk technique; ferrocene complex dissolved in CH2Cl2; PdCl2(cod) added in single portion, stirred for 20 min; react. mixt. evapd., Et2O added; ppt. filtered off, washed twice with hexane, dried in vac.; elem. anal.;
DOI:10.1002/ejic.201000365

Reference yield: 48.0%

: 1246383-83-4
(PPh₂C₅H₄)Fe(C₅H₄CHCHCOC₅H₄N)

: 26482-00-8
1-(2-oxo-2-(2-pyridyl)ethyl)pyridinium iodide

: 1246383-85-6
1-(diphenylphosphanyl)-1'-terpyridylferrocene

Guidance literature:: With ammonium acetate; In ethanol; under Ar, using Schlenk technique; Fe complex, ammonium acetate and C5H4NCOCH2C5H4NI dissolved in EtOH, heated for 3 h at reflux; react. mixt. allowed to cool to 25°C; ppt. filtered off, washed twice with ice-cooled EtOH; dried in vac.; elem. anal.;
DOI:10.1002/ejic.201000365