1-(4-methoxy-phenyl)-isochroman-3-one

Base Information

Chemical Name:1-(4-methoxy-phenyl)-isochroman-3-one
CAS No.:77605-67-5
Molecular Formula:C₁₆H₁₄O₃
Molecular Weight:254.285
Hs Code.:

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Chemical Property of 1-(4-methoxy-phenyl)-isochroman-3-one

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Technology Process of 1-(4-methoxy-phenyl)-isochroman-3-one

There total 4 articles about 1-(4-methoxy-phenyl)-isochroman-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50439-04-8
[2-(4-methoxy-benzoyl)-phenyl]-acetic acid

: 77605-67-5
1-(4-methoxy-phenyl)-isochroman-3-one

Guidance literature:: With platinized Raney nickel; Hydrogenation_.in alkal. Loesung und Behandlung des Reaktionsprodukts mit warmer wss. Salzsaeure;

Reference yield:

: 38199-92-7
3-(4-methoxyphenyl)-1H-indene

: 77605-67-5
1-(4-methoxy-phenyl)-isochroman-3-one

Guidance literature:: Multi-step reaction with 2 steps

1: 40 percent / K₂Cr₂O₇, concd H₂SO₄ / H₂O / 3 h / 55 °C

2: concd NH₄OH, Zn, CuSO₄ / H₂O / 72 h / Heating

With potassium dichromate; ammonium hydroxide; sulfuric acid; copper(II) sulfate; zinc; In water;
DOI:10.1021/jm00140a016

Reference yield:

: 100-66-3
methoxybenzene

: 77605-67-5
1-(4-methoxy-phenyl)-isochroman-3-one

Guidance literature:: Multi-step reaction with 2 steps

1: aluminium chloride / Isolierung ueber das durch Erhitzen auf 200grad erhaeltliche 3-<4-Methoxy-phenyl>-isocumarin, das mit Hilfe von wss. Natronlauge hydrolysiert wird.

2: platinized Raney nickel / Hydrogenation_.in alkal. Loesung und Behandlung des Reaktionsprodukts mit warmer wss. Salzsaeure

With aluminium trichloride; platinized Raney nickel;