trans-[PtCl₂(NH₃)(cyclohexylamine)]

Base Information

Chemical Name:trans-[PtCl₂(NH₃)(cyclohexylamine)]
CAS No.:174691-91-9
Molecular Formula:C₆H₁₆Cl₂N₂Pt
Molecular Weight:382.192
Hs Code.:

trans-[PtCl<sub>2</sub>(NH<sub>3</sub>)(cyclohexylamine)]

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Chemical Property of trans-[PtCl₂(NH₃)(cyclohexylamine)]

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Technology Process of trans-[PtCl₂(NH₃)(cyclohexylamine)]

There total 8 articles about trans-[PtCl₂(NH₃)(cyclohexylamine)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: potassium amminetrichloroplatinate

: potassium chloride

: 108-91-8,157973-60-9
cyclohexylamine

: 159701-67-4,99038-38-7,174691-91-9
cis-dichloro-trans-ammonia(cyclohexylamine)platinum

Guidance literature:: With KI; AgNO₃; In water; dropwise addn. of amine to mixt. of Pt-complex and KI, stirring for 1 h (pptn.), collection (filtration), washing (water), drying in air, dissoln. in water, treatment with AgNO3 (in dark, overnight), stirring with KCl at 40°C for 1 h; pptn. on standing at 4°C overnight, filtration, recrystn. (0.01 MHCl, 80°C);
DOI:10.1021/ic960983u

Reference yield: 80.0%

: 7647-01-0,15364-23-5
hydrogenchloride

: 15663-27-1
cisplatin

: 108-91-8,157973-60-9
cyclohexylamine

: 159701-67-4,99038-38-7,174691-91-9
trans-[PtCl₂(NH₃)(cyclohexylamine)]

Guidance literature:: In water; stirring Pt-complex with 2 equiv. of amine at 70°C, then refluxing, cooling to room temp., addn. of 12 M HCl, refluxing for 6 h; crystn. on cooling in ice, filtration, washing (H2O); elem. anal.;

Reference yield: 63.3%

: 7647-01-0,15364-23-5
hydrogenchloride

: C₆H₁₆ClIN₂Pt

: 159701-67-4,99038-38-7,174691-91-9
cis-dichloro-trans-ammonia(cyclohexylamine)platinum

Guidance literature:: C₆H₁₆ClIN₂Pt; With silver nitrate; In water; at 20 ℃; for 5h;

hydrogenchloride; In water; at 20 ℃;
DOI:10.1016/j.ica.2014.07.043