ReH₅(P(C₆H₅)3)2NH₂C₄H₉

Base Information

Chemical Name:ReH₅(P(C₆H₅)3)2NH₂C₄H₉
CAS No.:91229-73-1
Molecular Formula:C₄₀H₄₆NP₂Re
Molecular Weight:788.966
Hs Code.:

ReH<sub>5</sub>(P(C<sub>6</sub>H<sub>5</sub>)3)2NH<sub>2</sub>C<sub>4</sub>H<sub>9</sub>

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Chemical Property of ReH₅(P(C₆H₅)3)2NH₂C₄H₉

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Technology Process of ReH₅(P(C₆H₅)3)2NH₂C₄H₉

There total 1 articles about ReH₅(P(C₆H₅)3)2NH₂C₄H₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 12103-40-1
bis(triphenylphosphine)-rhenium heptahydride

: 75-64-9
tert-butylamine

: 91229-73-1
ReH₅(P(C₆H₅)3)2NH₂C₄H₉

Guidance literature:: In tetrahydrofuran; soln. of the Re-complex treated with the amine, refluxed for 10 min; solvent removed under vacuum, dried, crystd. from benzene/EtOH, elem. anal.;
DOI:10.1039/DT9860000067

Reference yield: 81.0%

: 67969-82-8
tetrafluoroboric acid diethyl ether

: 91229-73-1
ReH₅(P(C₆H₅)3)2NH₂C₄H₉

: 75-05-8,26809-02-9
acetonitrile

: 91229-75-3
ReH(NCCH₃)3(C₄H₉NH₂)(P(C₆H₅)3)2⁽²⁺⁾*2BF₄^(1-)

Guidance literature:: In acetonitrile; according to: Allison, J. D.; Walton, R. A. J. Chem. Soc., Chem. Commun. 1983, 401;;

Reference yield: 70.0%

: tetrafluoroboric acid

: 91229-73-1
ReH₅(P(C₆H₅)3)2NH₂C₄H₉

: 75-05-8,26809-02-9
acetonitrile

: 91229-75-3
ReH(NCCH₃)3(C₄H₉NH₂)(P(C₆H₅)3)2⁽²⁺⁾*2BF₄^(1-)

Guidance literature:: In diethyl ether; acetonitrile; byproducts: H2; (N2), suspn. of the Re-complex in CH3CN acidified with a soln. of HBF4 in Et2O (HBF4*Et2O); Et2O added, collected, recrystd. from CH2Cl2/Et2O in the presence of excess PPh3, collected, washed with Et2O, elem. anal.;
DOI:10.1039/DT9860000067