C₂₉H₃₂FNO₅

Base Information

Chemical Name:C₂₉H₃₂FNO₅
CAS No.:1362022-54-5
Molecular Formula:C₂₉H₃₂FNO₅
Molecular Weight:493.575
Hs Code.:

C<sub>29</sub>H<sub>32</sub>FNO<sub>5</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₉H₃₂FNO₅

Chemical Property:

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Technology Process of C₂₉H₃₂FNO₅

There total 6 articles about C₂₉H₃₂FNO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1362022-52-3
C₂₇H₂₈FN₃O₄

: 507-09-5
tiolacetic acid

: 1362022-54-5
C₂₉H₃₂FNO₅

Guidance literature:: With pyridine; at 20 ℃;
DOI:10.1039/c2cc17393j

Reference yield:

: 1235999-57-1
(2R,4aR,7R,8R,8aS)-6-(benzyloxy)-2-phenylhexahydropyrano[3,2-d][1,3]dioxine-7,8-diol

: 1362022-54-5
C₂₉H₃₂FNO₅

Guidance literature:: Multi-step reaction with 6 steps

1.1: pyridine / dichloromethane / 3 h / -20 - 0 °C

2.1: tetrabutylammoniun azide / toluene / 2.5 h / 65 - 100 °C

3.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 °C

3.2: 0 - 20 °C

4.1: triethylsilane; phenylborondichloride / dichloromethane / 1.5 h / -78 °C / Molecular sieve

4.2: -78 °C

5.1: diethylamino-sulfur trifluoride / dichloromethane / 72 h / -40 - 20 °C

6.1: pyridine / 20 °C

With pyridine; triethylsilane; diethylamino-sulfur trifluoride; phenylborondichloride; tetrabutylammoniun azide; sodium hydride; In dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1039/c2cc17393j

Reference yield:

: 100-39-0
benzyl bromide

: 1362022-54-5
C₂₉H₃₂FNO₅

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 °C

1.2: 0 - 20 °C

2.1: triethylsilane; phenylborondichloride / dichloromethane / 1.5 h / -78 °C / Molecular sieve

2.2: -78 °C

3.1: diethylamino-sulfur trifluoride / dichloromethane / 72 h / -40 - 20 °C

4.1: pyridine / 20 °C

With pyridine; triethylsilane; diethylamino-sulfur trifluoride; phenylborondichloride; sodium hydride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c2cc17393j