ClPtPh(PMe₂Ph)2

Base Information

Chemical Name:ClPtPh(PMe₂Ph)2
CAS No.:27081-34-1
Molecular Formula:C₂₂H₂₇ClP₂Pt
Molecular Weight:583.937
Hs Code.:

Synonyms:

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Chemical Property of ClPtPh(PMe₂Ph)2

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Technology Process of ClPtPh(PMe₂Ph)2

There total 2 articles about ClPtPh(PMe₂Ph)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 71035-52-4
platinum(II)(Cl)(η3allyl)(dimethylphenylphoshpine)

: 934-56-5
trimethyl(phenyl)stannane

: sym-{(platinum)2(phenyl)2(μ-Cl)2(dimethylphenylphosphine)2}

: 27081-34-1
trans-{platinum(Cl)bis(dimethylphosphine)}

Guidance literature:: In chloroform-d1; Under N2, a soln. of PtCl(C3H5(PMe2Ph) and Sn(CH3)3(C6H5) is placed in an NMR-tube.; Monitored by NMR, hexane is added to soln. in tube, pptn. of an off-white material, which is consisted of a mixt. of sym-trans/cis complexe.;

Reference yield:

: 880106-25-2
trans-[PtPh(O₃SCF₃)(PMe₂Ph)2]

: 56-34-8
tetraethylammonium chloride

: 27081-34-1
trans-{platinum(Cl)bis(dimethylphosphine)}

Guidance literature:: In dichloromethane-d2; (N2); Schlenk technique; Et4NCl was added to soln. of Pt complex in CD2Cl2;
DOI:10.1021/om051021a

Reference yield: 55.0%

: 27081-34-1
trans-{platinum(Cl)bis(dimethylphosphine)}

: 2923-28-6
silver trifluoromethanesulfonate

: 880106-25-2
trans-[PtPh(O₃SCF₃)(PMe₂Ph)2]

Guidance literature:: In dichloromethane; acetone; byproducts: Ag; (N2); Schlenk technique; soln. of Ag salt in acetone was added to stirred mixt. of Pt complex in CH2Cl2; soln. was shielded from light; reacted for 48 h; filtered; solvent removed; dried in vac. for 2 h; dissolved in C6H6; cooled at 4°C for 2 h; filtered; solvent removed; residue washed (petroleum ether); recrystd. (CH2Cl2/petroleum ether); elem. anal.;
DOI:10.1021/om051021a