FeCl(OC₆H₃(C₆H₃(CH₃)2)CHNCHC₆H₂(CH₃)3)2

Base Information

• Chemical Name: FeCl(OC₆H₃(C₆H₃(CH₃)2)CHNCHC₆H₂(CH₃)3)2
• CAS No.: 913063-04-4
• Molecular Formula: C₅₀H₅₀ClFeN₂O₂
• Molecular Weight: 802.259

Synonyms:

Chemical Property of FeCl(OC₆H₃(C₆H₃(CH₃)2)CHNCHC₆H₂(CH₃)3)2

Chemical Property:

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Technology Process of FeCl(OC₆H₃(C₆H₃(CH₃)2)CHNCHC₆H₂(CH₃)3)2

There total 1 articles about FeCl(OC₆H₃(C₆H₃(CH₃)2)CHNCHC₆H₂(CH₃)3)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

bis(3-xylylsalicylidene)-1,2-dimesitylethylenediamine (1027341-76-9) + iron(III) chloride (7705-08-0) → FeCl(OC6H3(C6H3(CH3)2)CHNCHC6H2(CH3)3)2 (913063-04-4)

Guidance literature:

In ethanol; addn. of ligand to a soln. of iron salt in ethanol, reflux for 30 min, standing at room temp.; recrystn. (acetonitrile); elem. anal.;

DOI:10.1021/ic060650p

Reference yield: 50.0%

methanol (67-56-1) + FeCl(OC6H3(C6H3(CH3)2)CHNCHC6H2(CH3)3)2 (913063-04-4) → Fe(OCH3)(OC6H3(C6H3(CH3)2)CHNCHC6H2(CH3)3)2*CH3OH

Guidance literature:

With NaOH; In methanol; water; addn. of aq. NaOH to a soln. of iron complex in methanol, stirring for 30 min at room temp.; filtration, recrystn. (pyridine/methanol); elem. anal.;

DOI:10.1021/ic060650p

Reference yield:

FeCl(OC6H3(C6H3(CH3)2)CHNCHC6H2(CH3)3)2 (913063-04-4) + water (7732-18-5) + silver perchlorate → Fe(H2O)(OC6H3(C6H3(CH3)2)CHNCHC6H2(CH3)3)2(1+)*ClO4(1-)*H2O=Fe(H2O)(OC6H3(C6H3(CH3)2)CHNCHC6H2(CH3)3)2ClO4*H2O

Guidance literature:

In tetrahydrofuran; addn. of a soln. of silver salt in THF to a soln. of iron complex in THF; filtration, evapn., dissolving in CH2Cl2, passing through teflon filter,recrystn. (CH2Cl2/hexane); elem. anal.;

DOI:10.1021/ic060650p

upstream raw materials:

bis(3-xylylsalicylidene)-1,2-dimesitylethylenediamine

iron(III) chloride

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