methyl 7-oxo-6-phenylthio-octanoate

Base Information

Chemical Name:methyl 7-oxo-6-phenylthio-octanoate
CAS No.:98711-86-5
Molecular Formula:C₁₅H₂₀O₃S
Molecular Weight:280.388
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 7-oxo-6-phenylthio-octanoate

Chemical Property:

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Technology Process of methyl 7-oxo-6-phenylthio-octanoate

There total 3 articles about methyl 7-oxo-6-phenylthio-octanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 67-56-1
methanol

: 98711-80-9
7-oxo-6-phenylthio-octanoic acid

: 98711-86-5
methyl 7-oxo-6-phenylthio-octanoate

Guidance literature:: With sulfuric acid; for 2h; Heating;
DOI:10.1039/P19850001237

Reference yield:

: 98711-81-0
2-acetyl-2-phenylthio-cyclohexanone

: 98711-86-5
methyl 7-oxo-6-phenylthio-octanoate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / H₂O; tetrahydrofuran / 20 h / Ambient temperature

2: 93 percent / cc H₂SO₄ / 2 h / Heating

With sodium hydroxide; sulfuric acid; In tetrahydrofuran; water;
DOI:10.1039/P19850001237

Reference yield:

: 931-59-9
benzenesulfenyl chloride

: 98711-86-5
methyl 7-oxo-6-phenylthio-octanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) sodium hydride / 1.) THF, room temp., 30 min 2.) THF

2: sodium hydroxide / H₂O; tetrahydrofuran / 20 h / Ambient temperature

3: 93 percent / cc H₂SO₄ / 2 h / Heating

With sodium hydroxide; sulfuric acid; sodium hydride; In tetrahydrofuran; water;
DOI:10.1039/P19850001237