2,3,5,6,7,8-Hexaaza-1,4-diphosphabicyclo(2.2.2)octane, 2,3,5,6,7,8-hexamethyl-

Base Information

• Chemical Name: 2,3,5,6,7,8-Hexaaza-1,4-diphosphabicyclo(2.2.2)octane, 2,3,5,6,7,8-hexamethyl-
• CAS No.: 3478-74-8
• Molecular Formula: C₆H₁₈N₆P₂
• Molecular Weight: 236.197
• DSSTox Substance ID: DTXSID50188327
• Nikkaji Number: J2.868.279D
• Wikidata: Q83060140
• Mol file: 3478-74-8.mol

Synonyms:2,3,5,6,7,8-Hexaaza-1,4-diphosphabicyclo(2.2.2)octane, 2,3,5,6,7,8-hexamethyl-;2,3,5,6,7,8-Hexaaza-1,4-diphosphabicyclo[2.2.2]octane, 2,3,5,6,7,8-hexamethyl-;3478-74-8;DTXSID50188327;2,3,5,6,7,8-hexamethyl-2,3,5,6,7,8-hexaaza-1,4-diphosphabicyclo[2.2.2]octane

Chemical Property of 2,3,5,6,7,8-Hexaaza-1,4-diphosphabicyclo(2.2.2)octane, 2,3,5,6,7,8-hexamethyl-

Chemical Property:

• Vapor Pressure: 0.124mmHg at 25°C
• Boiling Point: 218.7°C at 760 mmHg
• Flash Point: 86.1°C
• XLogP3: 1.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 0
• Exact Mass: 236.10681860
• Heavy Atom Count: 14
• Complexity: 178

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN1N(P2N(N(P1N(N2C)C)C)C)C

Technology Process of 2,3,5,6,7,8-Hexaaza-1,4-diphosphabicyclo(2.2.2)octane, 2,3,5,6,7,8-hexamethyl-

There total 4 articles about 2,3,5,6,7,8-Hexaaza-1,4-diphosphabicyclo(2.2.2)octane, 2,3,5,6,7,8-hexamethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

N,N'-Dimethylhydrazine dihydrochloride (306-37-6) + Hexamethylphosphorous triamide (1608-26-0) → tris(1,2-dimethylhydrazino)diphosphane (3478-74-8)

Guidance literature:

In toluene; for 72h; Reflux;

DOI:10.1002/zaac.201700106

Reference yield:

1,2-Dimethylhydrazine (540-73-8) → tris(1,2-dimethylhydrazino)diphosphane (3478-74-8)

Guidance literature:

With Hexamethylphosphorous triamide; In benzene; Heating;

Reference yield:

N,N'-Dimethylhydrazine dihydrochloride (306-37-6) → tris(1,2-dimethylhydrazino)diphosphane (3478-74-8)

Guidance literature:

With Hexamethylphosphorous triamide; In benzene; Heating;

upstream raw materials:

1,2-Dimethylhydrazine

3,6-Dichloro-1,2,4,5-tetramethyl-[1,2,4,5,3,6]tetrazadiphosphinane

N,N'-Dimethylhydrazine dihydrochloride

Hexamethylphosphorous triamide

Downstream raw materials:

N,N'-bis(dichlorophosphino)-N,N'-dimethylhydrazine

C₂₂H₃₄Cl₄N₁₁O₂P₅S₃

C₂₀H₂₈N₇O₄P₃S