C₃₅H₃₇ClF₂N₂O₃

Base Information

Chemical Name:C₃₅H₃₇ClF₂N₂O₃
CAS No.:1349024-62-9
Molecular Formula:C₃₅H₃₇ClF₂N₂O₃
Molecular Weight:607.14
Hs Code.:

C<sub>35</sub>H<sub>37</sub>ClF<sub>2</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:

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Chemical Property of C₃₅H₃₇ClF₂N₂O₃

Chemical Property:

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Technology Process of C₃₅H₃₇ClF₂N₂O₃

There total 8 articles about C₃₅H₃₇ClF₂N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1202647-32-2
C₄₀H₄₅ClF₂N₂O₅

: 1349024-62-9
C₃₅H₃₇ClF₂N₂O₃

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; dichloromethane; at 0 - 20 ℃;
DOI:10.1016/j.bmcl.2009.09.104

Reference yield:

: 143306-64-3
tert-butyl 8-oxo-5-azaspiro[2.5]octane-5-carboxylate

: 1349024-62-9
C₃₅H₃₇ClF₂N₂O₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: lithium diisopropyl amide / tetrahydrofuran

1.2: -78 °C

2.1: sodium hydride / tetrahydrofuran

3.1: bis-triphenylphosphine-palladium(II) chloride; sodium carbonate / water; N,N-dimethyl-formamide; isopropyl alcohol / 1 h / 80 °C

4.1: water; lithium hydroxide / tetrahydrofuran / 72 h / 60 °C

4.2: 20 °C

5.1: hydrogenchloride / 1,4-dioxane; dichloromethane / 0 - 20 °C

With hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride; water; sodium hydride; sodium carbonate; lithium hydroxide; lithium diisopropyl amide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; isopropyl alcohol; 3.1: Suzuki coupling;
DOI:10.1016/j.bmcl.2009.09.104

Reference yield:

: 851314-35-7
8-oxo-5-aza-spiro[2.5]octane-5,7-dicarboxylic acid 5-tert-butyl ester 7-methyl ester

: 1349024-62-9
C₃₅H₃₇ClF₂N₂O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / tetrahydrofuran

2.1: bis-triphenylphosphine-palladium(II) chloride; sodium carbonate / water; N,N-dimethyl-formamide; isopropyl alcohol / 1 h / 80 °C

3.1: water; lithium hydroxide / tetrahydrofuran / 72 h / 60 °C

3.2: 20 °C

4.1: hydrogenchloride / 1,4-dioxane; dichloromethane / 0 - 20 °C

With hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride; water; sodium hydride; sodium carbonate; lithium hydroxide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; isopropyl alcohol; 2.1: Suzuki coupling;
DOI:10.1016/j.bmcl.2009.09.104