(2,4-bis(2,6-diisopropylphenylimino)pent-3-yl)FePh

Base Information

Chemical Name:(2,4-bis(2,6-diisopropylphenylimino)pent-3-yl)FePh
CAS No.:944160-05-8
Molecular Formula:C₃₅H₄₆FeN₂
Molecular Weight:550.611
Hs Code.:

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Chemical Property of (2,4-bis(2,6-diisopropylphenylimino)pent-3-yl)FePh

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Technology Process of (2,4-bis(2,6-diisopropylphenylimino)pent-3-yl)FePh

There total 3 articles about (2,4-bis(2,6-diisopropylphenylimino)pent-3-yl)FePh which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: C₄₅H₆₇FeN₂NaO₅

: 944160-05-8
(2,4-bis(2,6-diisopropylphenylimino)pent-3-yl)FePh

Guidance literature:: With triphenylborane; Mechanism;
DOI:10.1038/s41586-020-2565-5

Reference yield: 67.0%

: 854669-50-4
[(2,4-bis(2,6-diisopropylphenylimino)pent-3-yl)Fe(μ-H)]2

: 960-71-4
triphenylborane

: 944160-05-8
(2,4-bis(2,6-diisopropylphenylimino)pent-3-yl)FePh

: 944160-03-6
(2,4-bis(2,6-diisopropylphenylimino)pent-3-yl)Fe(μ-H)2BPh2

Guidance literature:: In toluene; under N2; Fe complex and BPh3 dissolved in toluene; heated at 80°C for 18 h; volatiles removed under vac.; extd. with toluene; filtered; concd.; crystd. from pentane at -26°C (Fe-B complex); elem. anal.;
DOI:10.1021/om7003805

Reference yield: 63.0%

: (2-((2,6-diisopropylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)-pent-2-ene) lithium salt

: iron(II) chloride*1.5THF

: 100-59-4
phenylmagnesium chloride

: 944160-05-8
(2,4-bis(2,6-diisopropylphenylimino)pent-3-yl)FePh

Guidance literature:: In toluene; under N2; mixt. of Li salt of ligand and Fe complex in toluene stirred at 80°C for 22 h; PhMgCl in THF added; stirred at room temp. for 4h; solvent removed under vac.; extd. with pentane; filtered through Celite;concd.; crystd. at -45°C; elem. anal.;
DOI:10.1021/om7003805