2,6-bis[1-(2-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)phenylimino)ethyl]pyridine

Base Information

Chemical Name:2,6-bis[1-(2-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)phenylimino)ethyl]pyridine
CAS No.:1020071-98-0
Molecular Formula:C₃₃H₄₁B₂N₃O₄
Molecular Weight:565.328
Hs Code.:

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Chemical Property of 2,6-bis[1-(2-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)phenylimino)ethyl]pyridine

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Technology Process of 2,6-bis[1-(2-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)phenylimino)ethyl]pyridine

There total 1 articles about 2,6-bis[1-(2-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)phenylimino)ethyl]pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1129-30-2
2,6-Diacetylpyridine

: 191171-55-8
2-anilineboronic acid pinacol ester

: 1020071-98-0
2,6-bis[1-(2-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)phenylimino)ethyl]pyridine

Guidance literature:: In toluene; byproducts: H2O; (N2/Ar, Schlenk) a soln. of amine and pyridine-compound in toluene and molecular sieves were kept at 100°C for 3 days; filtered, the solvent was rotary evapd., recrystd. from ethanol; elem. anal.;
DOI:10.1021/om800036b

Reference yield: 92.0%

: 1020071-98-0
2,6-bis[1-(2-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)phenylimino)ethyl]pyridine

: iron(II) chloride

: 1020071-97-9
2,6-bis[1-(2-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)phenylimino)ethyl]pyridineiron(II) chloride

Guidance literature:: In tetrahydrofuran; (N2/Ar, Schlenk) FeCl2 was added to the soln. of pyridine-compound in THF, stirred for 12 h; ppt. was filtered, washed twice by pentane, dried at 1 mm vac.; elem. anal.;
DOI:10.1021/om800036b