C₂₉H₂₄NO₅PS

Base Information

Chemical Name:C₂₉H₂₄NO₅PS
CAS No.:1584736-78-6
Molecular Formula:C₂₉H₂₄NO₅PS
Molecular Weight:529.553
Hs Code.:

C<sub>29</sub>H<sub>24</sub>NO<sub>5</sub>PS

Synonyms:

Suppliers and Price of C₂₉H₂₄NO₅PS

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₉H₂₄NO₅PS

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of C₂₉H₂₄NO₅PS

There total 6 articles about C₂₉H₂₄NO₅PS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 92-29-5
hydrobenzamide

: 1584736-78-6
C₂₉H₂₄NO₅PS

Guidance literature:: Multi-step reaction with 6 steps

1.1: chloroform / Reflux

2.1: tetrahydrofuran / 4 h / 0 °C

3.1: ammonium hydroxide / water / 0.33 h / 20 °C

4.1: triethylamine; carbon disulfide / dichloromethane / 2 h / 0 °C

4.2: 2 h / 20 °C

5.1: 1-[3,5-bis(trifluoromethyl)phenyl]-3-[(1S,2S)-2-(dimethylamino)cyclohexyl]thiourea / toluene / 48 h / 30 °C

6.1: triethylamine / dichloromethane / 1 h / 20 °C

With carbon disulfide; 1-[3,5-bis(trifluoromethyl)phenyl]-3-[(1S,2S)-2-(dimethylamino)cyclohexyl]thiourea; ammonium hydroxide; triethylamine; In tetrahydrofuran; dichloromethane; chloroform; water; toluene;
DOI:10.1002/anie.201308514

Reference yield:

: 84044-04-2
diphenyl [1-(1-amino)benzyl]phosphonate

: 1584736-78-6
C₂₉H₂₄NO₅PS

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine; carbon disulfide / dichloromethane / 2 h / 0 °C

1.2: 2 h / 20 °C

2.1: 1-[3,5-bis(trifluoromethyl)phenyl]-3-[(1S,2S)-2-(dimethylamino)cyclohexyl]thiourea / toluene / 48 h / 30 °C

3.1: triethylamine / dichloromethane / 1 h / 20 °C

With carbon disulfide; 1-[3,5-bis(trifluoromethyl)phenyl]-3-[(1S,2S)-2-(dimethylamino)cyclohexyl]thiourea; triethylamine; In dichloromethane; toluene;
DOI:10.1002/anie.201308514

Reference yield:

: 100-52-7
benzaldehyde

: 1584736-78-6
C₂₉H₂₄NO₅PS

Guidance literature:: Multi-step reaction with 7 steps

1.1: ammonium hydroxide / water / 48 h / 20 °C

2.1: chloroform / Reflux

3.1: tetrahydrofuran / 4 h / 0 °C

4.1: ammonium hydroxide / water / 0.33 h / 20 °C

5.1: triethylamine; carbon disulfide / dichloromethane / 2 h / 0 °C

5.2: 2 h / 20 °C

6.1: 1-[3,5-bis(trifluoromethyl)phenyl]-3-[(1S,2S)-2-(dimethylamino)cyclohexyl]thiourea / toluene / 48 h / 30 °C

7.1: triethylamine / dichloromethane / 1 h / 20 °C

With carbon disulfide; 1-[3,5-bis(trifluoromethyl)phenyl]-3-[(1S,2S)-2-(dimethylamino)cyclohexyl]thiourea; ammonium hydroxide; triethylamine; In tetrahydrofuran; dichloromethane; chloroform; water; toluene;
DOI:10.1002/anie.201308514