5α,10β,15α,20β-tetrakis(2-aminophenyl)porphyrinatoiron(III) chloride

Base Information

Chemical Name:5α,10β,15α,20β-tetrakis(2-aminophenyl)porphyrinatoiron(III) chloride
CAS No.:97775-27-4
Molecular Formula:C₄₄H₃₂ClFeN₈
Molecular Weight:764.092
Hs Code.:

Synonyms:

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Chemical Property of 5α,10β,15α,20β-tetrakis(2-aminophenyl)porphyrinatoiron(III) chloride

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Technology Process of 5α,10β,15α,20β-tetrakis(2-aminophenyl)porphyrinatoiron(III) chloride

There total 1 articles about 5α,10β,15α,20β-tetrakis(2-aminophenyl)porphyrinatoiron(III) chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 52199-35-6
tetrakis-5,10,15,20-(o-aminophenyl)porphyrin

: 7647-14-5
sodium chloride

: 7789-46-0
iron(II) bromide

: 220457-32-9,743422-30-2,97775-27-4
5α,10β,15α,20β-tetrakis(2-aminophenyl)porphyrinatoiron(III) chloride

Guidance literature:: tetrakis-5,10,15,20-(o-aminophenyl)porphyrin; iron(II) bromide; With 2,6-dimethylpyridine; In tetrahydrofuran; at 20 ℃; for 4h; Inert atmosphere;

sodium chloride; In dichloromethane; water;
DOI:10.1021/jacs.6b07014

Reference yield: 79.0%

: 67-56-1
methanol

: 123-43-3
sulfoacetic acid

: 220457-32-9,743422-30-2,97775-27-4
5α,10β,15α,20β-tetrakis(2-aminophenyl)porphyrinatoiron(III) chloride

: 7732-18-5
water

: sodium 5α,10β,15α,20β-tetrakis(2-(sulfonatoacetamido)phenyl)porphyrinatoiron(III) hydroxide hexahydrate*3(methanol)

Guidance literature:: With isobutyl chlorocarbonate; triethyl amine; In dichloromethane; sulfoacetic acid added to soln. of isobutyl carbonate and Et3N; stirred at room temp. for 30 min; soln. of Fe compd. in CH2Cl2 added; stirred atroom temp. for 24 h; evapd. to dryness; dissolved in CHCl3; org. layer extd. (aq. NaOH); aq. layer washed (CHCl3); soln. evapd. to dryness; dissolved in EtOH; filtered; filtrate evapd.; purified by chromy. (Cosmosil 75C18-OPN, MeOH-H2O); evapd. to dryness;recrystd. (MeOH-ether); elem. anal.;
DOI:10.1016/j.ica.2004.01.038

Reference yield: 75.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 220457-32-9,743422-30-2,97775-27-4
5α,10β,15α,20β-tetrakis(2-aminophenyl)porphyrinatoiron(III) chloride

: chloro iron(III) α,β,α,β-5,10,15,20-tetra(o-N,N-dimethylaminophenyl)porphyrin

Guidance literature:: With sodium cyanoborohydride; acetic acid; In dichloromethane; water; acetonitrile; at 20 ℃; for 4h;
DOI:10.1021/jacs.6b07014