C₁₅H₁₃Cl₂NO₃

Base Information

Chemical Name:C₁₅H₁₃Cl₂NO₃
CAS No.:1285680-62-7
Molecular Formula:C₁₅H₁₃Cl₂NO₃
Molecular Weight:326.179
Hs Code.:

C<sub>15</sub>H<sub>13</sub>Cl<sub>2</sub>NO<sub>3</sub>

Synonyms:

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Chemical Property of C₁₅H₁₃Cl₂NO₃

Chemical Property:

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Technology Process of C₁₅H₁₃Cl₂NO₃

There total 8 articles about C₁₅H₁₃Cl₂NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 1285680-62-7
C₁₅H₁₃Cl₂NO₃

Guidance literature:: Multi-step reaction with 8 steps

1.1: potassium carbonate / acetone / Reflux

2.1: hydrogenchloride; iron / ethanol; water / Reflux

3.1: sulfuric acid / tetrahydrofuran / 0 °C

3.2: 0.5 h / 0 °C

3.3: 3 h / 0 °C / Reflux

4.1: copper(l) iodide; copper; potassium carbonate / 1-methyl-pyrrolidin-2-one / 40 h / 160 °C

5.1: 1.5 h / 105 °C

6.1: aluminum (III) chloride / 2.5 h / 160 - 250 °C / Inert atmosphere

7.1: water; sodium hydroxide / 2 h / Reflux

8.1: toluene-4-sulfonic acid / 3 h / 80 °C

With hydrogenchloride; aluminum (III) chloride; copper(l) iodide; sulfuric acid; water; iron; copper; potassium carbonate; toluene-4-sulfonic acid; sodium hydroxide; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; ethanol; water; acetone;
DOI:10.1016/j.cclet.2010.11.008

Reference yield:

: 100-17-4
para-methoxynitrobenzene

: 1285680-62-7
C₁₅H₁₃Cl₂NO₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: hydrogenchloride; iron / ethanol; water / Reflux

2.1: sulfuric acid / tetrahydrofuran / 0 °C

2.2: 0.5 h / 0 °C

2.3: 3 h / 0 °C / Reflux

3.1: copper(l) iodide; copper; potassium carbonate / 1-methyl-pyrrolidin-2-one / 40 h / 160 °C

4.1: 1.5 h / 105 °C

5.1: aluminum (III) chloride / 2.5 h / 160 - 250 °C / Inert atmosphere

6.1: water; sodium hydroxide / 2 h / Reflux

7.1: toluene-4-sulfonic acid / 3 h / 80 °C

With hydrogenchloride; aluminum (III) chloride; copper(l) iodide; sulfuric acid; water; iron; copper; potassium carbonate; toluene-4-sulfonic acid; sodium hydroxide; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; ethanol; water;
DOI:10.1016/j.cclet.2010.11.008

Reference yield:

: 696-62-8
para-iodoanisole

: 1285680-62-7
C₁₅H₁₃Cl₂NO₃

Guidance literature:: Multi-step reaction with 5 steps

1: copper(l) iodide; copper; potassium carbonate / 1-methyl-pyrrolidin-2-one / 40 h / 160 °C

2: 1.5 h / 105 °C

3: aluminum (III) chloride / 2.5 h / 160 - 250 °C / Inert atmosphere

4: water; sodium hydroxide / 2 h / Reflux

5: toluene-4-sulfonic acid / 3 h / 80 °C

With aluminum (III) chloride; copper(l) iodide; water; copper; potassium carbonate; toluene-4-sulfonic acid; sodium hydroxide; In 1-methyl-pyrrolidin-2-one;
DOI:10.1016/j.cclet.2010.11.008