Ru₃(carbonyl)10(triphenylphosphine)2

Base Information

Chemical Name:Ru₃(carbonyl)10(triphenylphosphine)2
CAS No.:116198-00-6
Molecular Formula:C₄₆H₃₀O₁₀P₂Ru₃
Molecular Weight:1107.9
Hs Code.:

Ru<sub>3</sub>(carbonyl)10(triphenylphosphine)2

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Chemical Property of Ru₃(carbonyl)10(triphenylphosphine)2

Chemical Property:

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Technology Process of Ru₃(carbonyl)10(triphenylphosphine)2

There total 12 articles about Ru₃(carbonyl)10(triphenylphosphine)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.3%

: 15243-33-1
dodecacarbonyl-triangulo-triruthenium

: 205441-17-4
Ru₃(CO)11(PPh₃)

: nonacarbonyltris(triphenylphosphine)triruthenium

: 116198-00-6,66172-60-9
{Ru3(CO)10(PPh3)2}

Guidance literature:: With triphenylphosphine; In cyclohexane; Ru3(CO)12 and PPh3 in 1:2 molar ratio were heated in cyclohexane at 55°C for 4 h under N2, reaction was monitored by IR spectroscopy; chromy. on silica gel, eluent light petroleum or benzene;
DOI:10.1016/0022-328X(83)85174-2

Reference yield: 66.0%

: 15243-33-1
dodecacarbonyl-triangulo-triruthenium

: chloro(η5-cyclopentadienyl)(triphenylphosphine)(η1-bis(diphenylphosphino)methane)ruthenium(II)

: 116198-00-6,66172-60-9
{Ru3(CO)10(PPh3)2}

Guidance literature:: In tetrahydrofuran; Ru-complex and Ru-complex were reacted in THF for 15 min under N2; solvent was removed in vac., evapd. of an acetone extract;

Reference yield: 48.0%

: 12120-15-9
ethylenebis(triphenylphosphine)platinum⁽⁰⁾

: Ru4(CO)13[μ3-PN((i)Pr)2]

: 116198-00-6,66172-60-9
{Ru3(CO)10(PPh3)2}

: [Ru3(CO)9Pt(CO)PPh3(μ4-PNiPr2)]

: [Ru4(CO)12Pt(CO)PPh3(μ4-PNiPr2)]

Guidance literature:: In tetrahydrofuran; Ru-complex and Pt-complex were dissolved in THF, stirred at room temp. for 24 h under N2; solvent was removed in vacuo, sepd. on TLC with hexane/CH2Cl2, crystd. from CH2Cl2-hexane at 28°C over several ds; elem. anal.;
DOI:10.1021/ic0106423