(5,5'-(1,3-propanediyldinitrilo)bis(1-phenyl-1,3-hexanedionato)^(4-))dicopper

Base Information Edit

Chemical Name:(5,5'-(1,3-propanediyldinitrilo)bis(1-phenyl-1,3-hexanedionato)^(4-))dicopper
CAS No.:66745-65-1
Molecular Formula:C₂₇H₂₆Cu₂N₂O₄
Molecular Weight:569.606
Hs Code.:
Mol file:66745-65-1.mol

(5,5'-(1,3-propanediyldinitrilo)bis(1-phenyl-1,3-hexanedionato)<sup>(4-)</sup>)dicopper

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Chemical Property of (5,5'-(1,3-propanediyldinitrilo)bis(1-phenyl-1,3-hexanedionato)^(4-))dicopper Edit

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Technology Process of (5,5'-(1,3-propanediyldinitrilo)bis(1-phenyl-1,3-hexanedionato)^(4-))dicopper

There total 2 articles about (5,5'-(1,3-propanediyldinitrilo)bis(1-phenyl-1,3-hexanedionato)^(4-))dicopper which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1469-95-0
1-phenylhexane-1,3,5-trione

: 6046-93-1
copper(II) acetate monohydrate

: 109-76-2,54018-94-9
Trimethylenediamine

: 66745-65-1
[5,11-dimethyl-1,15-diphenyl-6,10-diazapentadeca-4,11-diene-1,3,13,15-tetraonato^(4-)-N⁽⁶⁾N⁽¹⁰⁾O⁽³⁾O⁽¹³⁾;O⁽¹⁾O⁽³⁾O⁽¹³⁾O⁽¹⁵⁾]dicopper(II)

Guidance literature:: In ethanol; mixing 2 equiv. of triketone with 1 equiv. of diamine, heating on steam-bath for 15 min, addn. to hot soln. of 1 equiv. Cu(OAc)2, heating for 5 min (pptn.); cooling, collection (filtration), drying (vac., over silica gel); elem. anal.;
DOI:10.1039/DT9770002109

Reference yield:

: (OC(C₆H₅)CH₂COCH₂C(CH₃)N)2(CH₂)3

: 6046-93-1
copper(II) acetate monohydrate

: 66745-65-1
(5,5'-(1,3-propanediyldinitrilo)bis(1-phenyl-1,3-hexanedionato)^(4-))dicopper

Guidance literature:: With sodium methylate; In methanol; chloroform; soln. H4(BAA)2-1,3-pn and NaOCH3 in CH3OH and CHCl3 added dropwise to refluxing soln. Cu(OAc)2*H2O in CH3OH and refluxed overnight; solid recovered, washed with CH3OH and air-dried; elem. anal.;