[2,6-bis(tert-butoxymethyl)phenyl]diphenyltin chloride

Base Information

Chemical Name:[2,6-bis(tert-butoxymethyl)phenyl]diphenyltin chloride
CAS No.:770744-01-9
Molecular Formula:C₂₈H₃₅ClO₂Sn
Molecular Weight:557.748
Hs Code.:

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Chemical Property of [2,6-bis(tert-butoxymethyl)phenyl]diphenyltin chloride

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Technology Process of [2,6-bis(tert-butoxymethyl)phenyl]diphenyltin chloride

There total 1 articles about [2,6-bis(tert-butoxymethyl)phenyl]diphenyltin chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 2,6-bis(tert-butoxymethyl)phenyllithium

: 1135-99-5
diphenyltin(IV) dichloride

: 770744-01-9
[2,6-bis(tert-butoxymethyl)phenyl]diphenyltin chloride

Guidance literature:: In hexane; ligand in hexane was added dropwise to stirred suspn. of Sn-compound in hexane, heated for 5 h at 60°C, stirred overnight under Ar; solvent was evapd. in vacuo, dissolved in CHCl3, filtered, concd., layered with pentane, crystd.; elem. anal.;
DOI:10.1021/om020361i

Reference yield: 75.0%

: 770744-01-9
[2,6-bis(tert-butoxymethyl)phenyl]diphenyltin chloride

: 2966-50-9
silver trifluoroacetate

: [2,6-bis(tert-butoxymethyl)phenyl]diphenyltin trifluoroacetate

Guidance literature:: In dichloromethane; (Ar); standard Schlenk technique; Ag salt was added to stirred soln. of Sn compd. in CH2Cl2; mixt. was stirred at 25°C for 7 d; filtered; solvent evapd. (vac.); washed (pentane); elem. anal.;
DOI:10.1021/om049636f

Reference yield: 70.0%

: 770744-01-9
[2,6-bis(tert-butoxymethyl)phenyl]diphenyltin chloride

: 2923-28-6
silver trifluoromethanesulfonate

: 794537-51-2
[2,6-bis(tert-butoxymethyl)phenyl]diphenyltin trifluoromethansulfonate

Guidance literature:: In dichloromethane; (Ar); standard Schlenk technique; Ag salt was added to stirred soln. of Sn compd. in CH2Cl2; mixt. was stirred at 25°C for 7 d; filtered; solvent evapd. (vac.); washed (pentane); elem. anal.;
DOI:10.1021/om049636f