1-Allyl-cyclohexanecarbonyl azide

Base Information

Chemical Name:1-Allyl-cyclohexanecarbonyl azide
CAS No.:76403-25-3
Molecular Formula:C₁₀H₁₅N₃O
Molecular Weight:193.249
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Allyl-cyclohexanecarbonyl azide

Chemical Property:

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Technology Process of 1-Allyl-cyclohexanecarbonyl azide

There total 3 articles about 1-Allyl-cyclohexanecarbonyl azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 72335-83-2
1-allylcyclohexane-1-carboxylic acid chloride

: 76403-25-3
1-Allyl-cyclohexanecarbonyl azide

Guidance literature:: With sodium azide; In acetone; 1.) 0 deg C, 1 h, 2.) 25 deg C, 2 h;
DOI:10.1021/jo00321a017

Reference yield:

: 72335-50-3
1-(1-prop-2-enyl)cyclohexanecarboxylic acid

: 76403-25-3
1-Allyl-cyclohexanecarbonyl azide

Guidance literature:: Multi-step reaction with 2 steps

1: 2.104 g / thionyl chloride / 2 h / Heating

2: sodium azide / acetone; H₂O / 0.5 h

With thionyl chloride; sodium azide; In water; acetone;
DOI:10.1246/bcsj.76.1251

Reference yield:

: 98-89-5
Cyclohexanecarboxylic acid

: 76403-25-3
1-Allyl-cyclohexanecarbonyl azide

Guidance literature:: Multi-step reaction with 3 steps

1: lithium diisopropylamide / 1.) THF, 0 deg C, then 25 deg C, 1 h and 60 deg C, 0.5 h, 2.) 0 deg C, then 25 deg C, 16 h

2: thionyl chloride / 1 h / 25 °C

3: aq. sodium azide / acetone / 1.) 0 deg C, 1 h, 2.) 25 deg C, 2 h

With thionyl chloride; sodium azide; lithium diisopropyl amide; In acetone;
DOI:10.1021/jo00321a017