Technology Process of C9H9(2)HClNO2
There total 3 articles about C9H9(2)HClNO2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
N-chloro-succinimide; sodium pyrosulfate; trifluorormethanesulfonic acid; palladium diacetate;
In
1,2-dichloro-ethane;
at 20 ℃;
for 0.166667h;
Sealed tube;
DOI:10.1039/c3cc47431c
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: tert.-butyl lithium / diethyl ether / 3.75 h / 0 °C / Sealed tube
1.2: 0 - 20 °C / Sealed tube
2.1: potassium carbonate / acetonitrile / 4 h / Reflux; Sealed tube
3.1: N-chloro-succinimide; palladium diacetate; sodium pyrosulfate; trifluorormethanesulfonic acid / 1,2-dichloro-ethane / 0.17 h / 20 °C / Sealed tube
With
N-chloro-succinimide; sodium pyrosulfate; trifluorormethanesulfonic acid; tert.-butyl lithium; palladium diacetate; potassium carbonate;
In
diethyl ether; 1,2-dichloro-ethane; acetonitrile;
DOI:10.1039/c3cc47431c
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium carbonate / acetonitrile / 4 h / Reflux; Sealed tube
2: N-chloro-succinimide; palladium diacetate; sodium pyrosulfate; trifluorormethanesulfonic acid / 1,2-dichloro-ethane / 0.17 h / 20 °C / Sealed tube
With
N-chloro-succinimide; sodium pyrosulfate; trifluorormethanesulfonic acid; palladium diacetate; potassium carbonate;
In
1,2-dichloro-ethane; acetonitrile;
DOI:10.1039/c3cc47431c
