4-trimethylsiloxybutyrophenone

Base Information

• Chemical Name: 4-trimethylsiloxybutyrophenone
• CAS No.: 124468-98-0
• Molecular Formula: C₁₃H₂₀O₂Si
• Molecular Weight: 236.386
• Mol file: 124468-98-0.mol

Synonyms:

Chemical Property of 4-trimethylsiloxybutyrophenone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of 4-trimethylsiloxybutyrophenone

There total 1 articles about 4-trimethylsiloxybutyrophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,1,1,3,3,3-hexamethyl-disilazane (999-97-3) + succinylbenzene (2051-95-8) → 4-trimethylsiloxybutyrophenone (124468-98-0)

Guidance literature:

Multistep reaction;

DOI:10.1246/bcsj.63.1898

Reference yield:

4-trimethylsiloxybutyrophenone (124468-98-0) → tetrahydro-2-phenylfuran (16133-83-8)

Guidance literature:

With triethylsilane; tin(II) iodide; chloro-trimethyl-silane; antimonypentachloride; Yield given. Multistep reaction; 1) CH₂Cl₂, -78 deg C, 5 min, 2) CH₂Cl₂, -23 deg C, 2.5h;

DOI:10.1246/bcsj.63.1898

upstream raw materials:

1,1,1,3,3,3-hexamethyl-disilazane

succinylbenzene

Downstream raw materials:

tetrahydro-2-phenylfuran