N-{3-[(E)-3-(4-methoxyphenyl)acryloyl]-5-methyl-1,3,5-oxadiazinan-4-ylidene}nitramide

Base Information

Chemical Name:N-{3-[(E)-3-(4-methoxyphenyl)acryloyl]-5-methyl-1,3,5-oxadiazinan-4-ylidene}nitramide
CAS No.:1237740-63-4
Molecular Formula:C₁₄H₁₆N₄O₅
Molecular Weight:320.305
Hs Code.:

Synonyms:

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Chemical Property of N-{3-[(E)-3-(4-methoxyphenyl)acryloyl]-5-methyl-1,3,5-oxadiazinan-4-ylidene}nitramide

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Technology Process of N-{3-[(E)-3-(4-methoxyphenyl)acryloyl]-5-methyl-1,3,5-oxadiazinan-4-ylidene}nitramide

There total 3 articles about N-{3-[(E)-3-(4-methoxyphenyl)acryloyl]-5-methyl-1,3,5-oxadiazinan-4-ylidene}nitramide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 34446-64-5,42996-84-9
(E)-3-(4-methoxyphenyl)propenoyl chloride

: 153719-38-1
3,6-dihydro-3-methyl-N-nitro-2H-1,3,5-oxadiazin-4-amine

: 1237740-63-4
N-{3-[(E)-3-(4-methoxyphenyl)acryloyl]-5-methyl-1,3,5-oxadiazinan-4-ylidene}nitramide

Guidance literature:: With pyridine; In acetonitrile; for 8h; Reflux;
DOI:10.1002/cjoc.201180409

Reference yield:

: 943-89-5
(E)-3-(4-methoxyphenyl)acrylic acid

: 1237740-63-4
N-{3-[(E)-3-(4-methoxyphenyl)acryloyl]-5-methyl-1,3,5-oxadiazinan-4-ylidene}nitramide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 8 h / Reflux

2: pyridine / acetonitrile / 8 h / Reflux

With pyridine; thionyl chloride; In acetonitrile;
DOI:10.1002/cjoc.201180409

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 1237740-63-4
N-{3-[(E)-3-(4-methoxyphenyl)acryloyl]-5-methyl-1,3,5-oxadiazinan-4-ylidene}nitramide

Guidance literature:: Multi-step reaction with 3 steps

1: piperidine; pyridine / 1 h / Reflux

2: thionyl chloride / 8 h / Reflux

3: pyridine / acetonitrile / 8 h / Reflux

With piperidine; pyridine; thionyl chloride; In acetonitrile;
DOI:10.1002/cjoc.201180409