1,2-bis[(2,6-diisopropylphenyl)imino]acenaphthene germanium

Base Information

Chemical Name:1,2-bis[(2,6-diisopropylphenyl)imino]acenaphthene germanium
CAS No.:733810-42-9
Molecular Formula:C₃₆H₄₀GeN₂
Molecular Weight:573.317
Hs Code.:

Synonyms:

Suppliers and Price of 1,2-bis[(2,6-diisopropylphenyl)imino]acenaphthene germanium

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2-bis[(2,6-diisopropylphenyl)imino]acenaphthene germanium

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 1,2-bis[(2,6-diisopropylphenyl)imino]acenaphthene germanium

There total 2 articles about 1,2-bis[(2,6-diisopropylphenyl)imino]acenaphthene germanium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 10038-98-9
germaniumtetrachloride

: 153625-67-3
1,2-bis-[(2,6-diisopropylphenyl)imino]acenaphthene

: 733810-42-9
1,2-bis[(2,6-diisopropylphenyl)imino]acenaphthene germanium

Guidance literature:: With Na; In diethyl ether; byproducts: NaCl; vac.; Schlenk technique; ligand was reacted with Na in Et2O; GeCl4 was added by condensation in vac. to obtained suspn. at -30°C; warmed to ambient temp. with shaken; mixt. was stirred at 20°C for 1 h; volatiles removed in vac. at ambient temp. within 30 min; toluene added;heated to 70°c for 10 min; cooled to ambient temp.; centrifuged; decanted; concd. (vac.); elem. anal.;
DOI:10.1021/om0497846

Reference yield:

: 10038-98-9
germaniumtetrachloride

: 794458-05-2
N,N'-bis(2,6-diisopropylphenyl)acenaphthylene-1,2-diamine

: 733810-42-9
1,2-bis[(2,6-diisopropylphenyl)imino]acenaphthene germanium

Guidance literature:: N,N'-bis(2,6-diisopropylphenyl)acenaphthylene-1,2-diamine; With sodium; In tetrahydrofuran; for 24h; Inert atmosphere; Schlenk technique;

germaniumtetrachloride; In tetrahydrofuran; at 20 ℃; for 2h; Inert atmosphere; Schlenk technique;
DOI:10.1039/c9dt04652f

Reference yield: 47.0%

: 110-71-4
1,2-dimethoxyethane

: 733810-42-9
1,2-bis[(2,6-diisopropylphenyl)imino]acenaphthene germanium

: 7440-23-5
sodium

: C₁₂H₃₀NaO₆⁽¹⁺⁾*C₃₆H₄₁GeN₂^(1-)

Guidance literature:: 1,2-bis[(2,6-diisopropylphenyl)imino]acenaphthene germanium; sodium; In tetrahydrofuran; at 20 ℃; for 6h; Inert atmosphere; Schlenk technique;

1,2-dimethoxyethane;
DOI:10.1039/c9dt04652f