diiron(carbonyl)6(μ2-η2-CC(isopropyl))(μ-PPh2)

Base Information

Chemical Name:diiron(carbonyl)6(μ2-η2-CC(isopropyl))(μ-PPh2)
CAS No.:62475-91-6
Molecular Formula:C₂₃H₁₇Fe₂O₆P
Molecular Weight:532.052
Hs Code.:

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Chemical Property of diiron(carbonyl)6(μ2-η2-CC(isopropyl))(μ-PPh2)

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Technology Process of diiron(carbonyl)6(μ2-η2-CC(isopropyl))(μ-PPh2)

There total 1 articles about diiron(carbonyl)6(μ2-η2-CC(isopropyl))(μ-PPh2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.8%

: 17685-52-8
triiron dodecarbonyl

: 62199-59-1
(3-methyl-1-butynyl)diphenylphosphine

: 62475-91-6
diiron(carbonyl)6(μ2-η2-CC(isopropyl))(μ-PPh2)

Guidance literature:: With Me₃NO; In methanol; n-heptane; benzene; addn. of Me3NO in MeOH under stirring over 2 h to the Fe compd. and phosphine in heptane-benzene under dry N2, stirring for 1 h and heating for 2 h at 70°C; cooling to room temp., concn., column chromy. (Florisil), elution with heptane, concg. and storing at -10°C, elem. anal.;

Reference yield:

: 62475-91-6
diiron(carbonyl)6(μ2-η2-CC(isopropyl))(μ-PPh2)

: 139198-87-1
Fe₂(CO)4(P(C₆H₅)2)(CCCH(CH₃)2)((C₆H₅)2PCH₂)2

Guidance literature:: With bis(diphenylphosphino)ethane; In toluene; Schlenk line techniques, under N2; soln. of Fe-complex and phosphine stirred (10 min), temp. raised (to 50°C, further 1 h), cooled to room temp.; concn., stored (-10°C, 48 h); elem. anal.;

Reference yield:

: 62475-91-6
diiron(carbonyl)6(μ2-η2-CC(isopropyl))(μ-PPh2)

: 2071-20-7
bis-diphenylphosphinomethane

: 139198-85-9
Fe₂(CO)4(P(C₆H₅)2)(CCCH(CH₃)2)((C₆H₅)2PCH₂P(C₆H₅)2)

Guidance literature:: In toluene; Schlenk line techniques, under N2; soln. of Fe-complex and phosphine stirred (10 min), temp. raised (to 100°C), temp. maintained (1 h), cooled to room temp.; concn., stored (-10°C, 48 h); elem. anal.;