2-Bromo-N-cyclohexylaniline

Base Information

Chemical Name:2-Bromo-N-cyclohexylaniline
CAS No.:858516-27-5
Molecular Formula:C12H16BrN
Molecular Weight:254.17
Hs Code.:2921420090
DSSTox Substance ID:DTXSID10479086
Wikidata:Q72453905
Mol file:858516-27-5.mol

Synonyms:2-Bromo-N-cyclohexylaniline;858516-27-5;2-BROMO-N-CYCLOHEXYLBENZENAMINE;SCHEMBL3677154;DTXSID10479086;AKOS000240695

Suppliers and Price of 2-Bromo-N-cyclohexylaniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
2-Bromo-N-cyclohexylaniline 95+%
1g
$ 668.00

Chemenu
2-Bromo-N-cyclohexylaniline 95%
1g
$ 631.00

American Custom Chemicals Corporation
2-BROMO-N-CYCLOHEXYLANILINE 95.00%
5MG
$ 497.72

Alichem
2-Bromo-N-cyclohexylaniline
1g
$ 576.64

Total 14 raw suppliers

Chemical Property of 2-Bromo-N-cyclohexylaniline

Chemical Property:

PSA：12.03000
Density:1.355
LogP:4.26670
Storage Temp.:2-8°C
XLogP3:4.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:253.04661
Heavy Atom Count:14
Complexity:166

Purity/Quality:

97% ^*data from raw suppliers

2-Bromo-N-cyclohexylaniline 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCC(CC1)NC2=CC=CC=C2Br

Technology Process of 2-Bromo-N-cyclohexylaniline

There total 7 articles about 2-Bromo-N-cyclohexylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 615-36-1
2-bromoaniline

: 98-89-5
Cyclohexanecarboxylic acid

: 858516-27-5
2-cyclohexylamino-1-bromobenzene

Guidance literature:: With copper(I) thiophene-2-carboxylate; (4,4'-di-tert-butyl-2,2'-dipyridyl)-bis-(5-methyl-2-(4-fluorophenyl)pyridine(-1H))-iridium(III) hexafluorophosphate; N,N,N′,N′-tetramethyl-N″-tert-butylguanidine; bathophenanthroline; iodomesitylene diacetate; In 1,4-dioxane; at 20 ℃; for 1h; regioselective reaction; Inert atmosphere; Irradiation;
DOI:10.1038/s41586-018-0234-8

Reference yield: 65.0%

: 108-91-8,157973-60-9
cyclohexylamine

: 583-53-9
2,3-dibromobenzene

: 858516-27-5
2-cyclohexylamino-1-bromobenzene

Guidance literature:: With potassium fluoride on basic alumina; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; at 80 - 90 ℃; for 1h;
DOI:10.1055/s-2005-865241

Reference yield: 56.0%

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 615-36-1
2-bromoaniline

: 858516-27-5
2-cyclohexylamino-1-bromobenzene

Guidance literature:: With sodium tris(acetoxy)borohydride; acetic acid; In 1,2-dichloro-ethane; at 140 ℃; for 0.166667h; microwave irradiation;
DOI:10.1055/s-2006-949639