Technology Process of 5-iodo-2,3-dimethoxy-terephthalic acid dimethyl ester
There total 6 articles about 5-iodo-2,3-dimethoxy-terephthalic acid dimethyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: AgNO3; TFAA
2: H2 / Raney Ni
3: H(+); NaNO2; KI
With
hydrogen; hydrogen cation; silver nitrate; trifluoroacetic anhydride; potassium iodide; sodium nitrite;
nickel;
1: Crivello method / 3: Sandmeyer reaction;
DOI:10.1016/S0040-4039(01)00524-X
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 75 percent / HCl
2: 100 percent / K2CO3
3: AgNO3; TFAA
4: H2 / Raney Ni
5: H(+); NaNO2; KI
With
hydrogenchloride; hydrogen; hydrogen cation; potassium carbonate; silver nitrate; trifluoroacetic anhydride; potassium iodide; sodium nitrite;
nickel;
1: Fischer esterification / 3: Crivello method / 5: Sandmeyer reaction;
DOI:10.1016/S0040-4039(01)00524-X
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 100 percent / K2CO3
2: AgNO3; TFAA
3: H2 / Raney Ni
4: H(+); NaNO2; KI
With
hydrogen; hydrogen cation; potassium carbonate; silver nitrate; trifluoroacetic anhydride; potassium iodide; sodium nitrite;
nickel;
2: Crivello method / 4: Sandmeyer reaction;
DOI:10.1016/S0040-4039(01)00524-X
