N^γ-tert-butoxycarbonylbutyryl-β-benzyl-L-asparaginic acid α-amide

Base Information

Chemical Name:N^γ-tert-butoxycarbonylbutyryl-β-benzyl-L-asparaginic acid α-amide
CAS No.:129280-55-3
Molecular Formula:C₂₀H₂₉N₃O₆
Molecular Weight:407.467
Hs Code.:

N<sup>γ</sup>-tert-butoxycarbonylbutyryl-β-benzyl-L-asparaginic acid α-amide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N^γ-tert-butoxycarbonylbutyryl-β-benzyl-L-asparaginic acid α-amide

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Technology Process of N^γ-tert-butoxycarbonylbutyryl-β-benzyl-L-asparaginic acid α-amide

There total 1 articles about N^γ-tert-butoxycarbonylbutyryl-β-benzyl-L-asparaginic acid α-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 92762-94-2
β-benzyl-L-aspartic acid amide trifluoroacetate

: 69038-04-6
N-hydroxysuccinimide ester of 4-(tert-butoxycarbonylamino)butyric acid

: 129280-55-3
N^γ-tert-butoxycarbonylbutyryl-β-benzyl-L-asparaginic acid α-amide

Guidance literature:: With triethylamine; Yield given. Multistep reaction; 1.) DMF, 20 deg C, 20 min, 2.) a) 0 deg C, 1 h, b) 20 deg C, 1 d;
DOI:10.1007/BF00766860

Reference yield:

: 129280-55-3
N^γ-tert-butoxycarbonylbutyryl-β-benzyl-L-asparaginic acid α-amide

: 129300-79-4
N-tert-butoxycarbonyl-L-tryptophyl-γ-aminobutyryl-β-benzyl-L-asparaginic acid α-amide

Guidance literature:: Multi-step reaction with 2 steps

1: 0.31 g / CH₂Cl₂ / 0.5 h / 20 °C

2: 1.) Et₃N / 1.) DMF, 20 deg C, 20 min, 2.) a) 0 deg C, 1 h, b) 20 deg C, 1 d

With triethylamine; In dichloromethane;
DOI:10.1007/BF00766860