1-phenyl-6,7-dihydro-1H-indazol-4(5H)-one

Base Information

• Chemical Name: 1-phenyl-6,7-dihydro-1H-indazol-4(5H)-one
• CAS No.: 14823-31-5
• Molecular Formula: C₁₃H₁₂N₂O
• Molecular Weight: 212.251
• European Community (EC) Number: 877-374-4
• DSSTox Substance ID: DTXSID80406228
• Nikkaji Number: J1.795.153J
• Wikidata: Q82211125

Synonyms:1-phenyl-6,7-dihydro-1H-indazol-4(5H)-one;14823-31-5;1-phenyl-6,7-dihydro-5H-indazol-4-one;1-phenyl-1,5,6,7-tetrahydro-4H-indazol-4-one;1-PHENYL-1,5,6,7-TETRAHYDRO-INDAZOL-4-ONE;SCHEMBL2512530;DTXSID80406228;PSXCLWPFIRHOJO-UHFFFAOYSA-N;HMS1606B11;STK235451;AKOS000320434;1,5,6,7-tetrahydro-1-phenyl-4h-indazol-4-one;EN300-7441255;1-Phenyl-1,5,6,7-tetrahydro-4H-indazole-4-one;1-phenyl-4,5,6,7-tetrahydro-1H-indazol-4-one;Z223646134

Chemical Property of 1-phenyl-6,7-dihydro-1H-indazol-4(5H)-one

Chemical Property:

• XLogP3: 2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 1
• Exact Mass: 212.094963011
• Heavy Atom Count: 16
• Complexity: 273

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CC2=C(C=NN2C3=CC=CC=C3)C(=O)C1

Technology Process of 1-phenyl-6,7-dihydro-1H-indazol-4(5H)-one

There total 11 articles about 1-phenyl-6,7-dihydro-1H-indazol-4(5H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

2-(dimethylaminomethylene)cyclohexane-1,3-dione (85302-07-4) + phenylhydrazine hydrochloride (59-88-1) → 4-Oxo-1-phenyl-4,5,6,7-tetrahydrobenopyrazole (14823-31-5)

Guidance literature:

With hydrogenchloride; In water; isopropyl alcohol; at 65 - 70 ℃;

DOI:10.1016/j.tetlet.2014.04.058

Reference yield: 91.0%

1,3-cylohexanedione (504-02-9) + N,N-dimethyl-formamide dimethyl acetal (4637-24-5) + phenylhydrazine (100-63-0) → 4-Oxo-1-phenyl-4,5,6,7-tetrahydrobenopyrazole (14823-31-5)

Guidance literature:

With 2,2,2-trifluoroethanol; for 1h; regioselective reaction; Reflux;

DOI:10.1016/j.jfluchem.2011.07.014

Reference yield: 90.0%

2-(dimethylaminomethylene)cyclohexane-1,3-dione (85302-07-4) + phenylhydrazine (100-63-0) → 4-Oxo-1-phenyl-4,5,6,7-tetrahydrobenopyrazole (14823-31-5)

Guidance literature:

In acetic acid; butan-1-ol; for 2h; Heating;

upstream raw materials:

2-(dimethylaminomethylene)cyclohexane-1,3-dione

phenylhydrazine

phenylhydrazine hydrochloride

1,3-cylohexanedione

Downstream raw materials:

thiosemicarbazone de la tetrahydro-1,5,6,7 phenyl-1 indazolone

5-bromo-4-oxo-1-phenyl-4,5,6,7-tetrahydroindazole

1-phenyl-4-oxiranylmethoxy-1H-indazol

4-Hydroxyethylidene-1-phenyl-4,5,6,7-tetrahydrobenzopyrazole

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 14823-31-5 1-phenyl-6,7-dihydro-1H-indazol-4(5H)-one

Send

Send

Metric Ton KG G Pound L ML

Send

Send